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GCMS analysis results for sample AD26626, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26626 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031940–000031967

Folder label: “GCMS X 11/7/01 A 12/6/01

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Scanned page image, NYC-WTC_000031950
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Furan, tetrahydro-2-(methoxyme Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.11 1.46 ng/uL 449470 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Furan, tetrahydro-2 - (methoxymethyl) 116 C6H1202 019354-27-9 45 2 Propanoic acid, 2-methyl-, anhydrid 158 C8H14O3 000097-72-3 40 3 2-Hepten-3-ol, 4,5-dimethyl- 142 C9H180 055956-37-1 38 4 Cyclopentanol , l-methyl- 100 C6H120 001462-03-9 36 Abundance 7 Scan 139 (6.113 min): 26626.D (-) m/ z 71.05 100.00% 7|1

5000 43

............ ... 5.80 6.00 6.20 6.40 'm/z-> 10 20 30 — 40 51760. I701' 50 80 90 100 100 110 120 130 m/ Z 43.05 45.32% 'Abundance #64310: Furan, tetrahydro-2-(methoxymethyl)- 71

43 5000 5.80 6.00 6.20 6.40___ _ m/z 41.0,5 24.17% 58 !........ 85 ....................... 116............... TI3I ———————— m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance I #11901: Propanoic acid, 2-methyl-, anhydride

43 71 K —A 5.80 6.00 6.20 6.40 5000- m/ Z 42 . ( 20.95%

27 37 , 55 ■ ■ i • ' i ■ ■ ' ■ i ' ' ' ' i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #8051: 2-Hepten-3-ol, 4,5-dimethyl- Af T. । 71 5.80 6.00 6.20 6.40 m/ z 3 9.1.0 10.43% 5000 43

4 27 i 15 I • • i • ■ ■ > i • ■ ■ • । ■ • ■ ■ । ■ 55 1 I 1 ' i ■ ' ■ ' i ' ,i Tel 81 100 — ——— , , j , ! TTPTmpT 109 124 'm/z- 10 2G 30 40 50 60 70 80 90 100 110 120 130 5.80

26626.D NP112701.M Fri Dec 07 14:50:05 2001 Page 5

NYC-WTC_000031950

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