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GCMS analysis results for sample AD26626, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26626 identifying unknown compounds on December 10, 2001.

NYC-WTC_000031940–000031967

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26626.D Vial: 3 Acq On 6 Dec 2001 11:59 am Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Pentanol, 5-amino- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

5.65 0.55 ng/uL 168860 1,4-Dichlorobenzene-d4 11.89

Hit# Of 5 entative ID MW MolForm CAS# Qual

1 Pentanol, /5-amino - 103 C5H13NO 002508-29-4 4 2 2-Butanamine, (S) - 73 C4H11N 000513-49-5 4 3 N-Ethylformamide 73 C3H7NO 000627-45-2 4 4 1,3 -Butanediamine 88 C4H12N2 000590-88-5 4 Abundance Scan 89 (5.655 min): 26626.D (-) m/z 40.00 100.00%| 40 44 5000

5.40 5.60 5.80 6.00 i 36 TH H— 57 71 85 — HT p-m TTTTTTHTTTTTTTTTTTTTT m/ z 44.00 57.60% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #1829: Pentanol, 5-amino- 30 AV 5000 5.40 5.60 5.80 6.00 m/z 41.00 12.10% ,4,3. 5659 67 72 86 V*0‘000—uM—uuuuunun3ur m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #301: 2-Butanamine, (S)- 44

5.40 A 5.60 5.80 6.00 5000 m/ z 4 5.10 11.29%

27 30 58 1 39 . 55 72 m/z-> 'Abundance 5 10 15 20 ‘T '''' i' 25 30

30 TOWpu]u*ummum—)uupanpUHTTTTTPT 35 40 45 50 55 60 65 #292: N-Ethylformamide 70 75 80 85 90

5.40 N 5.60 5.80 6.00 73 m/z 43.05 10.25% 5000 44 58 27

mii 15 - T’ET 5 10 15 20 25 30 35 4C —41— 5 11" " I" ' i " " i " " i " 11' "' i " " ITTTTTT 50 55 60 65 70 75 80 85 90 5.40 5.60 5.80 6.00

26626.D NP112701.M Fri Dec 07 14:50:03 2001 Page 4

NYC-WTC_000031949

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NYC-WTC_000031949Source: NYC Law Department, mirrored locally

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