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Document / 344 pages

DEP GCMS data table, Jan-Feb 2002

Machine-extracted title · confidence 90%

Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004149–000004492

Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02

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Scanned page image, NYC-WTC_000004443
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30707.D Vial: 41 Acq On : 29 Dec 2001 10:35 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

7.61 2.51 ug/1 1090490 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1-Butanamine, 3-methyl- _ _ 87 C5H13N ___ 000107-85-7 9 Abundance Scan 279 (7.609 min): 30707.D (-) m/z. 7 3 .00 ’10 0.0 0 % 73

5000 43

m/z-> I" " 11H'I -mm .II55 । Hp 87 103 207 " r "1 r11' i “ " r " ■ r'" r "' i" " i" " r "11' ■" r ■" r "' i"' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.20 m/ z 7.40 43.05 7.60 7.80 8.00 32.32% (Abundance #63573: 3-Pentanol, 3-methyl- 73

5000

J 7.20 7.40 7.60 7.80 8.00 55 m/ z 41.05 12.08% 45 87 27 i , ... .............. ,1...................................................................... ‘ ‘‘‘14" 11'"' ।‘ ।...11. i.. ।.... । < 11.11>।>11 > । > 1111 > 11.1111■।<11 ■ । ■ । > 11111111j111111111111111111 m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance 26200 ■ 13-Diovelane, 2-mitn 73

7.20 7.40 7.60 7.80 8.00 5000 43 m/ z 45.0,5 11.80% 58 27 87 TTT TpTTTp7T7Trrrrp-rTriTTTTpnnn7TTTTpTTTpjTTpT-rrpnnn^^ m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 == ., I ■. Abundance #292: N-Ethylformamide 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.0.0 7.26% 5000 44 58 15 ! - m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 7.20 7.40 7.60 7.80 8.00 |

30707.D GCMS1126.M Mon Jan 28 11:23:44 2002 Page 1

NYC-WTC_000004443

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NYC-WTC_000004443Source: NYC Law Department, mirrored locally

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