GCMS analysis report for sample AE01232, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1802\1232.D Vial: 39 Acq On : 18 Feb 2002 3:07 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.36 ug/1 25795 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 2 1,3-Dioxolane 74 C3H602 000646-06-0 7 3 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 5 4 1-Butanamine , 2-methyl - 87 C5H13N 000096-15-1 5 Abundance Scan 345 (8.207 min): 1232.D (-) m/z 73.00 100.00% 73

5000 43 ■ ■ i ■ ■

87 7.80 8.00 8.20 8.40 8.60 ....................... 111/49 ............ PT 103 m/z 43.05 29.01% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73 — 5000 - 7.80 8.00 8.20 8.40 8.60 55 m/z 40.95 12.08% 27 45 87 ■ ' i ■ ■ ■ ‘ i ‘ I 3?,. 1 ■ i ' ■ ■ ■ i ■ ' ■ ■ i ‘ ‘ ■ i ■ 1 1 ■ i ‘ 1. .1 . miz—__ 10 20 30 40 50 60 70 80 90 100 110 Abundance 73 ........ AAA....... I * ‘ 1 ‘ 1 ' ’ ' * 1 ‘ ‘ ‘ 1*’’I* 29 44 7.80 8.00 8.20 8.40 8.60 5000 m/ z 44.9,5 10.05%

.....................................36................................................................................................. mfe-> ___ 10____ 20____ 30 40 50 60 70 80 90____ 100___110 Abundance #62527: Formamide, N,N-dimethyl- ~ ~ ........ 44 73 7.80 8.00 8.20 8.40 8.60 m/z 71.00 6.51% 5000 30 15 39, 58 * > I • • i t i ■ ■ ■ ■ । I • ' i ■ ■ ‘ ■ i ‘ ■ TTI 1 1 ■ i ■ ' ‘ ' i ■ ' ■ ■ i ' ■ ' ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1232.D GCMS0208.M Thu Feb 21 09:34:07 2002 Page 1

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