GCMS analysis results for sample AE02567, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR1902\2567.D Vial: 22 Acq On : 21 Mar 2002 1:42 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.15 0.34 ug/1 41760 1,4-Dichlorobenzene-d4 12.26 / Hit# of 5 I Tentative ID MW MolForm CAS# Qual 1 3-Pentanol,/ 3-methyl- 102 C6H140 000077-74-7 28 2 Formamide, /N,N-dimethyl- 73 C3H7NO 000068-12-2 5 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 1, 3-Dioxolane 74 C3H602 000646-06-0 4

A Abundance Scan 338 (8.150 min): 2567.D (-) m/ z 73.00 100.00% 73

5000 43 "II 1 ' ' ' I ' 1 1 ' 1 1 1 1 1 1 1 7.80 8.00‘ ‘8.20 “ 8.40______ .......................... i 1,1,1 , 51 57....... ,| 1 1 1 1 ' 1 1 I > I I I I I I I I I 1 11 I [ I J'I I I I I I I I I , I 84 , ' ■ l - ' ■' । l > - ■ 103 ■ l ■' । । • l > m/ z 42.95 32.16% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 .. .... UL... _ 7.80 8.00 8.20 8.40 _ 55 m/z 45.05 11.50% 45 87 27 1 ' 39, |) TT — ' i 1 ' ■ ' 1 1 ' ' r 1 -------- m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 44 73 ' ' i ■ ■ 1 ■ i ■ 1 ■ ‘ i ‘ ' i ■ 7.80 8.00 8.20 8.40_______ 5000 m/ z 41.05 9.42% 30 15 39 58 TI <'•’>'> TFIIT 1Pr m/z-> Abundance 10 20 30 40 50 60 #292: N-Ethylformamide 70 80 90 100 110 A.. . LA— ' 1 t ' • ' ■ i ' 30 7.80 8.00 8.20 8.40 73 m/ z 70.9,0 8.71% 5000 44 58

15 —.......... rT T T* * T TT 44 1 ' ' l 'I I | I ! । ■ ■ ■ ■ ) ■ 1 • ■ । ■ ■ • ■ । 1 > ] 1 ■ ■ 1 । ' । 1 1 i 1 1 1 1 i 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 I 7.80 8.00 .20 8.40

2567.D GCMS0308.M Thu Mar 21 14:20:01 2002 Page 1

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