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GCMS analysis results for sample AE02567, March 2002

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AE02567 conducted on March 25, 2002, identifying other unknown compounds.

NYC-WTC_000038901–000038910

Folder label: “GCMS X 3/4/02 A 3/20/02

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Scanned page image, NYC-WTC_000038909
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR1902\2567.D Vial: 22 Acq On : 21 Mar 2002 1:42 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 1.79 ug/1 290523 Naphthalene-d8 15.91

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 47 2 PhenethylAmine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 38 3 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benzeneethanamine, N-[ (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1069 (14.861 min): 2567h (-) ].. m/z..... 72.9,5 100.00% 73

5000 267 355 ................. \.................... , 45 103 125 154 193 223 249 k 293 323 14.60 14.80 15.00 15.20 “I ""l—00—00000——TTT TTmuuUMgOgur m/ z 2 67.00 42.74% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420440 | Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 -...............— 5000 14.60 14.80 15.00 15.20 m/z 355.05 38.51% 207 249 | 323 .. ............................................. < ।> i > J > 1111111111 > 111 n 111111. ] i 111 i r> | i" " i' ■" i'" I—IEII—IEUIUITETIT m/Z-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance .. ■_ ' : ’ 73 ...................... 14.60 14.80 15.00 15.20 5000 355 m/ z 356.05 14.04% 44 147 193 267294 m/z->... 40 60 80 100120140160180200220240260280 300320 340 360380400420440 Abundance #57357: Noradrenaline, tetra-TMS -...............— 73 ____ 14.60 14.80 15.00 15.20 m/z 268.00 10.98% 5000 102 355

45 147 1 442 —..... 4............ m/z-> 40 60 80 100120140160180200220240260280300320 340 360380400420440 14.60 14.80 15.00 15.20

2567.D GCMS0308.M Thu Mar 21 14:20:05 2002 Page 2

NYC-WTC_000038909

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NYC-WTC_000038909Source: NYC Law Department, mirrored locally

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