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GCMS analysis results, Sample AE08434, April 18, 2002

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GCMS analysis report for sample AE08434 showing surrogate recovery and unknown compound screening on April 18, 2002.

NYC-WTC_000048550–000048560

Folder label: “GCMS X 4/10/02 A 4/15/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\APR1202\8434.D Vial: 23 Acq On : 16 Apr 2002 5:38 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.82 0.55 ug/1 93235 Naphthalene-d8 15.86 Hit# of 5 Tentative ID MW MolForm CAS# Qual

I Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 0 0 0 5 41-02 - 6 (87) 2 Noradrenaline,/tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 3 Phenethylamine, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 4 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 32 Abundance 7 Scan 1065 (14,824 min): 8434.D (-) m/ z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 103 133154 193 223 323 J ‘ 'I •1" * i m/ z 2 67.00 39.04% m/z—> 50 100 150 200 250300 350 400 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000- 14.40 14.60 14.80 15.00 15.20 m/z 355.05 38.57% 207 323 I IInnYm n/z-> 50 100 150 200 250 300 350 400 Abundance #57357: Noradrenaline, tetra-TMS 73

14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 12.34% 102

45 | 147 442 ‘ 'I ' 1 m/z-> 50 100 150 200 250 300 350 400 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris(trimethyls 73 1 1 1 1 1 1 1 ' 1 1 1 1 1 14.40 14.60 14.80 15.00 15.20 m/z 268.00 10.76%

5000 355 44

ili 147 193 267 294 K rfm ‘ 'i 1 1 ‘ ' i ' 1 ' 1 i ' '' ' '' i 1 ' ' ■ i ■ ' 1 1 i ■ m/z-> 50 100 150 200 250 300 350 400 14.40 14.60 14.80 15.00 15.20

8434.D GCMS0412.M Wed Apr 17 09:48:00 2002 Page 3

NYC-WTC_000048559

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NYC-WTC_000048559Source: NYC Law Department, mirrored locally

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