GCMS analysis results for sample AE02579, March 2002

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Data File : C:\HPCHEM\l\DATA\MAR1902\2579.D Vial: 28 Acq On : 21 Mar 2002 7:39 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.87 0.45 ug/1 83423 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 91 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38 3 N- (Trifluoroacetyl) -N,O,O' ,0' 1 -tetr 553 C22H42F3NO4Si4 000000-00-0 37 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance " ... * Scan 1070 (14.866 min): 2579.D (-) m/z. 73.00 100.00% 73

267 5000 355 ........ - 45 14.60 14.80 15.00 15.20 — 125 154 191 , , 237 । 3231 m/z 267.00 53.52% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000- 267 —........ / ............. — _____ 14.60 14.80 15.00 15.20 m/z 355.05 47.87% 1......... 207 . i 323, ' ' i 1 ' 1 ' i ■ ■' ■ '' i 1 1 ' 1 1 1 ' ' ' i 1 ' ‘ 1 i 1 1 1 1 1 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 — 14.60 14.80 15.00 15.20 267 5000 179 m/ z 3 56.05 17.98% 356 45 147 209 237 312 m/z-> _ 50 _100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacety)-N,O,O’,0"-tetrakis(trimethylsi —................ 73 14.60 14.80 15.00 15.20 m/z 2 67.90 13.11% 355 500G

45 1 147 193 267 I 538 - 1 ' i ' ' ' ' i ' ' ' ' i ■ ‘ ' i ' 1 ■ ' i ' 1 m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

2579.D GCMS0308.M Thu Mar 21 14:28:56 2002 Page 2

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