GCMS analysis results for sample AE06998, April 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\l\DATA\APR0405\6998.D Vial: 27 Acq On 6 Apr 2002 11:30 pm Operator: Sample gc/ms scan 3/26 fb Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.84 1.59 ug/1 121094 Naphthalene-d8 15.88 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 N- (Trifluoroacetyl) -N,O,O' ,O' '-tetr 553 C22H42F3NO4Si4 000000-00-0 47 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 43 4 Noradrenaline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 Abundance ' Scan 1067 (14.841 min): 6998. D (-) m/z 73.00 100.00% 73

5000 267 355

45 14.60 14.80 15.00 15.20 125 154 193 2371 . — 1I|'।II |I।I I|I IIr , Tl 1 323 [ m/z 267.00 42.94% mz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 J 118 14.60 14.80 15.00 15.20 m/z 355.05 39.66% 207 , 1 323 m/z--> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60162: N-(Trifluoroacetyl)-N,O,O',O"-tetrakis(trimethylsi 73 1 1 i 1 ■ • i 1 1 355 14.60 14.80 15.00 15.20 5000 m/z 356.05 13.73%

45 LL 147 193 267 [ 538 1 'I ■ ' T ‘ t ' ‘ TIT 1 T ' * i • > T T t TT 1r • T I TT I I TT "t 1 I I I 1 I T I I I I I |T T

mlz-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 14.60 14.80 15.00 15.20 m/z 268.00 12.04%

5000-

45 | | 208 251 281 | 386 458 548 ■ 1 [ ■ 1 ■ ■ I ■ ■ ■ ■ I ' < ■ ■ I 1 । 1 f i'> f i j । । 1 ■ I ■ ■ ■ • i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ TTITT ■ ■ i ■ ■ m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

6998.D GCMS0408.M Mon Apr 15 14:45:07 2002 Page 1

NYC-WTC_000040086