GCMS surrogate recovery data for sample AE07636, April 2002

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Data File : C:\HPCHEM\1\DATA\APRI102\7636.D Vial: 12 Acq On : 12 Apr 2002 1:12 am Operator: Sample : gc/ms scan 4/3 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 Cyclopentasiloxane, decamethyl Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 14.83 0.62 ug/1 88514 Naphthalene-d8 15.87 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 3 N-(Trifluoracetyl)-0,0',0"-tris(tri 495 C20H36F3NO4Si3 000000-00-0 38 4 Phenethylamine , N-methyl-.beta. ,3,4 399 C18H37NO3Si3 010538-85-9 38 Abundance Scan 1066 (14.828 min): 7636.D (-) m/z 73.00 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20 4 1 i 125 154 193 223 . 323 1 1 T 'i1 r ' + ' T—— I Tt | —— J ] I I I I J I T T I I I I J I I I T m/z 267.00 40.38% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 1 1 ’ ' 1 1 1 1 14.40 14.60 14.80 15.00 15.20 m/ z 355.05 40.01% 207 | 323 11 1 TIT ——— —1 n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 355 TIT/I/EEI111 TtTI 1 1 1 TLI 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.05 15.30%

45 I , 1...... ' ' i ' ■ ' 1 208 i 251 281 f ' 1 I —T TIT 386 458 548 m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #58807: N-(TrifIuoracetyl)-O,O',O‘'-tris(trimethylsilyl)epin 1 1 i ■ 1 73 14.40 14.60 14.80 15.00 15.20 355 m/z 268.00 13.19% 5000

45 140 184 281 | 11l h 480 1 m/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

7636.D GCMS0412.M Thu Apr 18 10:49:22 2002 Page 1

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