Laboratory report documenting GCMS analysis of sample AE08019 conducted on April 24, 2002, including surrogate recovery data.
NYC-WTC_000047734–000047743Folder label: “GCMS X 4/4/02 A 4/12/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\APR1102\8019.D Vial: 25 Acq On : 12 Apr 2002 1:59 pm Operator: Sample : gc/ms scan 4/4 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
14.83 0.78 ug/1 120172 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl - 370 C10H30O5Si5 000541-02-6 64 2 Benzoic acid, 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 37 3 Benzeneethanamine, N- (pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 4 Phenethylami , N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 37 Abundance Scan 1066 (14.829 min): 8019.D (-) m/ z 73.00 100.00% 73
5000 267 355
14.40 14.60 14.80 15.00 15.20 45 — 125 154 193,223 , k 323 ..... m/z 267.00 45.43% m/z->____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 ....... ,.......... 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 42.65% 207 323, — nz->____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #73975: Benzoic acid, 2,4-bis[(trimethylsilyl)oxy]-, trimet 73 ........ /......... 14.40 14.60 14.80 15.00 15.20 5000 355 m/z 356.05 14.57% 45
133 193 223 281 । r i I > > । > i । < '| 1 i > r | 1 ii । | i h i1' । । । । i i |" i > , । i i i i । i i i i । i i , i । i r
m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 73 14.40 14.60 14.80 15.00 15.20 355 m/z 267.90 11.78% 5000
45 | | 208 251 281 386 458 548 ' 1 I ' ' ' . । । . . . ! . . , i- | . . . ( , ■ । TC—B,m—n—m——m—TT , ............................. ................. nz—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20
8019.D GCMS0412.M Tue Apr 16 12:08:48 2002 Page 2
NYC-WTC_000047742
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Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
NYC-WTC_000049167
Laboratory report documenting GCMS analysis of sample AE08836 conducted on April 25, 2002, showing detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049360
Laboratory report documenting GCMS analysis of sample AE08932 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049320
Laboratory report documenting GCMS analysis of sample AE08840 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049350
Laboratory report documenting GCMS analysis of sample AE08931 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049147
Laboratory report documenting GCMS analysis of sample AE08834 conducted on April 25, 2002, showing detection of unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000046673
Laboratory report documenting GCMS analysis of sample AE07318 conducted on April 10, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048857
GCMS laboratory report for sample AE08682 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000048867
GCMS laboratory report for sample AE05683 analyzed on April 23, 2002, by analyst DLV.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049370
Laboratory report documenting GCMS analysis of sample AE08933 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049380
Laboratory report documenting GCMS analysis of sample AE08935 conducted on April 26, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040088
Laboratory report documenting GCMS analysis of environmental sample AE06997 conducted on April 16, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000040146
Laboratory report documenting GCMS analysis of sample AE06991 conducted on April 16, 2002, including surrogate recovery data.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000047639
Department of Environmental Protection GCMS analysis record dated April 4-12, 2002.
Filed in the same folder
NYC-WTC_000047640
Fragmented page from a GCMS record dated April 12, 2002, containing method parameters and sample identifiers.
Filed in the same folder
NYC-WTC_000047643
Laboratory report of a GCMS blank analysis for sample AE08012 conducted on April 17, 2002, showing non-detect levels for various compounds.
Filed in the same folder
NYC-WTC_000047652
Laboratory report of GCMS calibration data for sample AE08012 conducted on April 17, 2002, listing target compounds and concentrations.
Filed in the same folder
NYC-WTC_000047656
Laboratory report of GCMS reference analysis for sample AE08012 conducted on April 17, 2002, showing recovery percentages for target compounds.
Filed in the same folder