GCMS sample analysis results for unknowns, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\1\DATA\MAY0802\9579.D Vial: 16 Acq On 9 May 2002 1:15 am Operator: Sample RE-EXT. Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.79 2.36 ug/1 188842 Naphthalene-d8 15.83 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 2 Benzoic/acid, 2,5-bis(trimethylsilo 370 370

3 Benzeneethanamine, N-[ (pentafluorop 563 4 3 ,4-Dihydroxybenzyl alcohol, tris (tr 356 C10H3005Si5 C16H30O4Si3 000541-02-6 003618-20-0 C24H34F5NO3Si3 055429-13-5 38 C16H3203Si3 068595-79-9 37 6 Abundance Scan 1064 (14.792 min): 9579.D (-) m/z 73.10 100.00%

5000 267 355 V TT 1 I ' ' 1 1 I ' 1 45 14.40 14.60 14.80 15.00 15.20 108 154 193 223 323 1 1 1 'i ‘ II- | m/z 267.05 32.41% m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000 267 J Tlt 14.40 14.60 14.80 15.00 15.20 m/z 355.10 29.32%

PIm— ——:323,..................................................... 207 m/z-> 50 100 150 200 250 300) 350 400 450 500 550 Abundance #73978: Benzoic acid, 2,5-bis(trimethylsiloxy)-, trimethyls 73 . -- -i । 355 14.40 14.60 14.80 15.00 15.20 5000 m/z 356.10 10.01%| 45

t ] । । । 147 179 223 267 297 > । i । । । ] । । r 1 । 1 t i । i i i i 1 I i t । i i i i । । । । ।—। ।—।—i ।—।—i—r 1 'i m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #74706: Benzeneethanamine, N-[(pentafluorophenyl)methylene] 1 i ' ' TT 73 14.40 14.60 14.80 15.00 15.20 355 m/z 74.10 8.77%

5000

45 208 251 281 386 458 548 ", 1 1 I-1 | ' i i i i | । । i r' | r f I I I 1 I 1 [ I I 1 1 n ■ 1 ■1 i 1 1 ■ ' i 1 1 ' 1 i 1 1 1 11 1 1 11. n/z—> 50 100 150 200 250 300 350 400 450 500 550 14.40 14.60 14.80 15.00 15.20

9579.D GCMS0507.M Fri May 10 08:21:58 2002 Page 2

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