GCMS analysis results for sample AE02576, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR1902\2576.D Vial: 25 Acq On : 21 Mar 2002 4:40 am Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 1.43 ug/1 284148 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H30O5S15 000541-02-6 91 2 Phenethylamine, N-methyl-.beta. , 3,4 399 C18H37NO3Si3 010538-85-9 38 3 Benzeneethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 32 4 Benzoic acid 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 32 Abundance Scan 1069 (14.863 min): 2576.D (-) m/ z 73.00.... 100.00% 73

5000 267 355 ......... —......... 45 125 154 193 223 _____ 14.60 14.80 15.00 15.20 .1 1 I 293 323. | TTI 1 1 ' "I TT 1'' 1 i'1 111 ' 1 ‘ ’ i ' ' i“ m/ z 267.00 47.17% m/Z"> 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 5000- 267 .............................. .................. 14.60 14.80 15.00 15.20 m/z 355.05 44.31% 207 T-r 1 T — i ——323 — Tu—nma—n—/I—B-mmTTT m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 -...... 14.60 14.80 15.00 15.20 5000- 355 m/ z 356.05 16.34% 44 147 193 267 294 ' ' i ' ' ' ' TT ' T i ' ' ‘ ' i ' ' ' * i 1 —— 1——}————— , , TIT m/z-> 50 100 150 200 250 300 350 400 450 500 550 —......4.......... Abundance #74706: Benzeneethanamine, N-[(pentafiuorophenyijmethyiene] 73 355 14.60 14.80 15.00 15.20 m/ z 2 68.00 12.98% 5000

45 208 251 281 1 386 458 548 \ ' 1 J T 1 ■ ■ ............... —T । 1 1 ■^r1 1 1 1 i 1 1 m/z~> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20

2576.D GCMS0308.M Thu Mar 21 14:25:18 2002 Page 2

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