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← Document results/DEP Box 57/GCMS X 3/7/02 A 3/27/02
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GCMS analysis page, sample AE01153, March 2002

Machine-extracted title · confidence 100%

Laboratory report page showing surrogate recovery data for sample AE01153 analyzed on March 22, 2002.

NYC-WTC_000058798–000058815

Folder label: “GCMS X 3/7/02 A 3/27/02

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Scanned page image, NYC-WTC_000058813
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB2102\1153.D Vial: 66 Acq On 24 Feb 2002 9:02 am Operator: Sample gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.93 1.00 ug/1 66233 Naphthalene-d8 15.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 87 2 Benzoic acid,/2-[(trimethylsilyl)ox 282 C13H22O3Si2 003789-85-3 38 3 Phenethylamihe, N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 4 Benzeneethahamine, N-[(pentafluorop 475 C21H26F5NO2Si2 055429-85-1 28 Abundance i '■ Sca'n l 077 (T4.927 min): iT53.D"(-)‘... ~........... ...... ... ......... ............. ...... I m/ z 73.00 100.00% 7)3

5000 267 355

45 223 251 14.60 14.80 15.00 15.20 I 133 1 54 177 193 323 339 m I”' ' ' ' I ' ' ‘ ' I TjVTTTp-i+rp+rq- m/z 267.00 41.15% ni/z~> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #51266: Cyclopentasiloxane, decamethyl- J 713

355 267 5000 14.60 14.80 15.00 15.20 m/z 355.0,5 34.18% 191 207 251 323 339 I A i I '' '' I m-rp-r I ’' '' I ___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #72300; Benzoic ac;d. 2-[(trirnei.hyteilyi)oxyj-, tnmethylsi 73 i ' I __ 14.60 14.80 15.00 15.20 267 m/z 356.0,5 13.05% 5000

45 92 ^f^isi 175 193 209 233 249 I ni/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tris{trimethyls ■’"T 7(3 14.60 14.80 15.00 15.20 m/z 268.00' 11.56% 5000 355 44

im/z-> X I, 88 40 60 130 147 193 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 267 294 14.60 14.80 15.00 15.20

1153.D GCMS0208.M Fri Mar 08 14:33:18 2002 Page 2

NYC-WTC_000058813

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NYC-WTC_000058813Source: NYC Law Department, mirrored locally

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