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GCMS analysis page, sample AE01153, March 2002

Machine-extracted title · confidence 100%

Laboratory report page showing surrogate recovery data for sample AE01153 analyzed on March 22, 2002.

NYC-WTC_000058798–000058815

Folder label: “GCMS X 3/7/02 A 3/27/02

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Scanned page image, NYC-WTC_000058812
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB2102\1153.D Vial: 66 Acq On : 24 Feb 2002 9:02 am Operator: Sample : gc/ms scan 2/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 4.51 ug/1 233541 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H14O ' 000077-74-7 28 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 28 3 Butane, 2 -/methoxy-2 -methyl - .102 C6H14O 000994-05-8 9 4 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 9 Abundance "7 ■ Scan 344 (8.l‘9iB miri): 1153.D (-) m/ z 73.00 100.00% 1 i .! 713 ! 5000 43

87 7.80 8.00 8.20 8.40 31} I, I 35 I I 103 i m/z 43.0,5 30.99% m/Z”> 10 20 30 40 50 70 60 80 90 100 110 'Abundance #63571 iPentanoi, 3-methyi- 7|3

5000 7.80 8.00 8.20 8.40 8.60 55 m/z 44.95 11.98% 45 I 87 27 I . 39, I I ' I ' ' ' ' I ' 10 20 30 40 50 60 70 80 90 100 110 'Abundance #845; Silane, tetrarnediyl- 73 .................. ............................ 7.80 8.00 8.20 8.40 8.60 5000 m/z 41.05 11.45%

45 15 31 55 ...........68........... I ' ' ' ' I ' ' ' ‘ I ' ' ’ ' I ' ' ' ' I ' ' ' ' I ' 'ni/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- ............ 713 7.80 8.00 8.20 8.40 8.60 m/z 7.00% 5000 55 87 97 • 45 ..... ? 33 ■ V L . I ' I ' ' ' ' I ' ' ' ' I ' ' ‘ ‘ I ' 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1153.D GCMS0208.M Fri Mar 08 14:33:13 2002 Page 1

NYC-WTC_000058812

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NYC-WTC_000058812Source: NYC Law Department, mirrored locally

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