GCMS sample AE05064 analysis, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR3002\5063.D Vial: 35 Acq On : 31 Mar 2002 2:41 am Operator: Sample : gc/ms scan 3/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 0.56 ug/1 75969 1,4-Dichlorobenzene-d4 12.25

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol,/ 3-methyl- 102 C6H14O 000077-74-7 9 2 Pentane, 37methoxy- 102 C6H14O 036839-67-5 9 3 2-Butanone/, 3-methoxy-3-methyl- 116 C6H12O2 036687-98-6 9 4 Butane, 2-(methoxy-2-methyl- 102 C6H14O 000994-05-8 9 Abundance ...... .. ..... . .. Scan 336(8.133min):5063.b{-) ’ • 7l3 .m/z...73T0jD~"~i0d70^

5000 43

39 57 7.80 8.00 __8.20 __840___ ...... ...... 1^^ .... Uhl.......... .... m/z 43.05 30.67% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63573: 3-Pentano(, 3-methyi- 45

5000 __ 7.80 8.00 8.20 8.40 ____ 55 m/z 45.05 11.02% ?7 87 ft )n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1793: Pentane, 3-metl’oxy- 7.3 ...... 7.80 8.00 8.20 8.40____ 5000 m/ z 41.05 10.88% 45

'm/z->___ 20 25 30 35 40 45 50 55 60 65 70.75_80__85___90 95 100 105 110 'Abundiance #3263:2-Butandne,’3-methoxy-3-iTi'ethyl- I ' 7)3 _2:8L_8:00__a20__840^__ m/z 71.00 7.55% 43 5000

........ !\,.... .. .... [J, ... 57 85 101 'm/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 | 7^80 8.00 8.20 8.40

5063.D GCMS0308.M Tue Apr 02 15:36:43 2002 Page 1

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