GCMS analysis results for sample AE02761, Mar 11, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2761.D Vial: 16 Acq On 1 Mar 2002 11:07 pm Operator: Sample gc/ms scan 2/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.30 ug/1 24162 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 4 4 1,3-Dioxolane, 2-pentadecyl- 284 C18H36O2 004360-57-0 4 Abundance / Scan 344 (8.200 min): 2761.D (-) m/z... 73.00....100.00% 73

5000 43 7.80 8.00 8.20 8.40 8.60

m/z-> 39 mTTTTTTTTTTT 49—4+ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 m/z 42.95 27.76% 87 ' i " " i " " r 1'' i " " i ■

Abundance #63573: 3-Pentanoi, 3-methyl- 73

5000 7.80 8.00 8.20 8.40 8.60 55 m/ z 45.0.5 10.21% — 45 87 27 31 41 TTIWTUTLWWT)WTTTIWTITTTUITTTTTT ■ ■ i ■1 69 84 ■ ir'" I'11' i' " ' i ■ " ' i " " I " " i " " i' m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance i 30 73 7.80 8.00 8,20 8.40 8.60 5000 m/z 41.05 10.04% 44 58 27 15 41 ■ ■'' । ।1''■।1''■।'11 ■ ■ ‘ ■ i ■ । ■1 ■11 ■ “ ■ ।'1' ।' ■ ■ ■। ■'■■।'1'11 ■ ■■' i ■ ■' ■ ।' ■' ■ । ‘ । •' ■ ■ ।' m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62884: 1-Butanamine, 3-methyl- 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.54% 5000

27 4144 55 59 70 73 87 TIIWTWLWTTTTTTTH+ —mmmmmmmmm 1.—0—I0100031100——BIT m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60 j

2761 .D GCMS0208.M Tue Mar 05 10:46:32 2002 Page 1

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