GCMS analysis results for sample AE02602, Mar 2002

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Data File C:\HPCHEM\l\DATA\MAR0102\2602.D Vial: 12 Acq On 1 Mar 2002 7:11 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 2 09 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.36 ug/1 28203 1,4-Dichlorobenzene-d4 12.31

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 36 2 Formamide, N, N-dimethyl - 73 C3H7NO 000068-12-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 1,3-Dioxolane 74 C3H602 000646-06-0 4 Abundance l Scan 344 (8.198 min): 2602.D (-) ; m/z 73.0.0 100.0 0% 3

5000 43 1 i ■ ■ ' 1 i ' ■ 1 ' । ■ 111) ' ■ ■ ' । ■ ■

m/z-> 4 51 55 ..... 34871111/01 THTTTTT 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 69 7.80 m/ z 8.00 43.05 8.20 8.40 _ 28.69% 8.60

Abundance #63573: 3-Pentanoi, 3-methyl- 73

A 5000 7.80 8.00 8.20 8.40 8.60 _ 55 m/ z 44.95 13.19% — 27 31 41 45 | "lnu!un01‘1——u—a——- TTTWUTTIWTTTIWTTTIWTTIWTWWIPTTTT 69 i, 848/ m/z-? 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance . ..... 44 73

7.80 8.00__ 8.20 8.40 8.60 5000 m/z 41.05 10.54% 30 15 27 3841 58 TTVImuuuppau m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 - Abundance #763: 1-Butanamine, 3-methyl- 30 7.80 8.00 8.20 8.40 8.60 m/z 70.90 6.89% 5000-

15 2/ 4144 55 55 70 87 TIITTTTOTTTTT TIOTTm—muuhTg m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60 :

2602.D GCMS0208.M Mon Mar 04 11:46:20 2002 Page 1

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