Laboratory report documenting GCMS analysis of sample AE01643 conducted on March 4, 2002, including surrogate recovery data.
NYC-WTC_000010167–000010175Folder label: “GCMS X 1/25/02 A 2/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB2502\1643 .D Vial: 5 Acq On : 25 Feb 2002 2:37 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
8.20 0.30 ug/1 22997 1,4-Dichlorobenzene-d4 12.32
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 Formamide, N,N-dimethyl - 73 C3H7NO 000068-12-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 N-Ethyl formamide 73 C3H7NO 000627-45-2 5 Abundance Scan 344 (8.197 min): 1643.D (-) 73 m/z 73.00... 100.00%
5000 43 r l 1 1 ' ‘ 1 ' —PPPP 7.80 8.00 8.20 8.40 8.60
m/z-> ■■i•■•■। 449 7+ ..... 8487.... m/z 42.95 ■i•■•■।»j" 39 i • > • 11 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 30.46% Abundance #63573: 3-Pentanol, 3-methyl- 73
5000 ■ i • ■ ■ 1 i • ■ ■ ■ i ■ ‘ ■ ‘i ■ * ■ * । » 7.80 8.00 8.20 8.40 8.60 55 m/ z 41.05 12.58% 45 27 31 41 69 1’1—001—0200—3—201/007 " ■ ■ i —00—| —"—— 84 87 *—— m/z— 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 44 73
7.80 8.00 8.20 8.40 8.60 5000 m/z 45.05 10.98% 30 15 “ “ 1 ' ‘ " 1 ‘ ‘ ‘ 27 ‘ 1 ' ‘ 3841 58 ‘ I “ ' ‘ ......................... I “ ' .. ............. । i < 1 . । i i । । . । I | I | i i ) i i i r-pn-r i [ . ) i 1 | i < i . | i m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #763: 1-Butanamine,3-methyl-................ *.... ......... ......... 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 7.30% 5000
m/z-> -H 15 27 ,4144 5558 70 T’1m—10001—001100071—20u002uu 87 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60
1643.D GCMS0208.M Thu Feb 28 09:29:06 2002 Page 1
NYC-WTC_000010174
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NYC-WTC_000010205
Laboratory report documenting GCMS analysis of sample AE01688 conducted on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010187
Laboratory report documenting GCMS analysis of sample AE01651 conducted on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009860
Analytical results for sample AE01436 analyzed via GCMS on March 6, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010232
Laboratory report documenting GCMS analysis of sample AE01691 conducted on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000009825
Analytical results for sample AE01329 analyzed via GCMS on March 5, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010196
Laboratory report documenting GCMS analysis of sample AE01687 conducted on March 4, 2002, including surrogate recovery data.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058339
Gas chromatography-mass spectrometry analysis of environmental sample AE04802 conducted April 4, 2002, detecting unknown compounds and surrogates.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038130
Laboratory report listing detection results for volatile organic compounds in sample AD31498 analyzed on February 27, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000006328
Initial GCMS analysis report for sample AE03435 conducted by analyst DLV on March 12, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000038149
Laboratory report listing detection results for volatile organic compounds in sample AD31549 analyzed on February 27, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000058382
Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04591.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059499
Reference analysis report for sample AE05701 conducted on April 5, 2002, quantifying recovery of specific organic compounds.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000010146
Administrative record from DEP Box 14 covering the period of January to February 2002 regarding World Trade Center environmental activities.
Filed in the same folder
NYC-WTC_000010147
Administrative header page for the GCMS folder covering samples from late January through late February 2002.
Filed in the same folder
NYC-WTC_000010150
Laboratory report of a GCMS blank run on February 28, 2002, showing non-detect levels for various target compounds.
Filed in the same folder
NYC-WTC_000010158
Calibration record for GCMS analysis conducted on February 28, 2002, listing response factors for target analytes.
Filed in the same folder
NYC-WTC_000010162
Laboratory report of GCMS analysis of reference standards on February 28, 2002, verifying instrument performance.
Filed in the same folder