GCMS analysis results for sample AE01436, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1436.D Vial: 8 Acq On : 21 Feb 2002 9:00 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.35 ug/1 25236 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual -------------------- ---- ------------------------- 1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 28 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 4 Formamide, N, N-dimethyl- 73 C3H7NO 000068-12-2 5 Abundance Scan 345 (8.209 min): 1436.D (-) m/z 73.00 “. 100.00% 73

5000 43 i . (

391 । 49 7.80 8.00 8.20 8.40 8.60 j —WImOPTITTTMTTTTT TmmmH55 69. 84 87 1WIWPI m/z-> .5. 10. 15. 20 25 30. 35. 40. 45. 50. 55. 60 65 70 75 80. 85 90. 95 m/z 42.95 30.17% Abundance #63573: 3-Pentanoi, 3-methyl- 73

5000 ...... 4...... 7.80 8.00 8.20 8.40 8.60 55 m/z 41.05 12.03% , 27 31 41 45 87

mz-> —mmTTTTTTT 1'1 H 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 69

Abundance ..................' .................. -...... 30 73 P............ 8.60 7.80 8.00 8.20 8.40 5000 m/z 44.95 10.40% 44 58 27 15 41 ■ “ ■ । ■ ■ ■' ।। ।■ ■■ ■। "i“"। ■i “ “। । “111 “1 ■ ।■ "i" " ।"11111" i11 ■1111" i" m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #763:1-Butanamine, 3-methyl- 30 7.80 8.00 8.20 8.40 8.60 m/z 71.00 8.45% 5000

15 27 ,4144 55 58 70umamng 87 —TTT - 1‘001u —0—nfummnT — m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8,20 8.40 8.60

1436.D GCMS0208.M Fri Feb 22 09:31:32 2002 Page 1

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