GCMS analysis results for sample AE01329, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1329.D Vial: 5 Acq On : 21 Feb 2002 6:01 pm Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.33 ug/1 23340 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 5 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 4 Abundance Scan 345 (8.207 min): 1329.D (-) m/z 73.00. 100.00% 73

5000 43 ............................... ............. . ..............■!. 87 103 7.80 8.00 8.20 8.40 8.60 f > > j 1 » ■ *-r J > i i i j i1' > । । i m/z 43.05 29.42% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol. 3-methyl- 73 .... ........... .

5000 7.80 8.00 8.20 8.40 8.60 55 m/z 40.95 12.22% 45 87 27 39, 1 '.......................... 1 , ■ ■ i ' ' ■ 1 i ' ' ■ ■ i ‘ ■ 1 ■ i ■ • ■ • i ' ' 40 50 i ■ ■ ■ ■ i ■ 60 70 1. 80 ,1 90. 100 110 m/z-_ __ 10 _ _ _ _____ 3Q _ Abundance 30

7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 11.60%

15 41 55 70 87 1 ‘ I ‘ 1 ' 1 I 1 ‘ ‘ i ‘ ‘ ' I ' 1 ■ ■ i ■ ■ ' ■ i ‘ ■ I ' 1 1 1 I 1 1 I 1 1 1 1 I 1 ' 1 1 I 1 miz-2 10 20 30 40 50 60__ 70___ 80___ 90 100 110 Abundance #292: N-Ethylformamide i ' ' ‘ ■ i ‘ 1 1 ‘ 1 ' ‘ 1 • i ■ ■ ■ ■ i ■ 1 33 7.80 8.00 8.20 8.40 8.60 73 m/ z 71.00 8.43% 5000 44 58

15 m/z-> 1 10 20 30 : 1 1 I 40 ■ । 50 ‘ i ■ ■ ■ ■ i ■ 1 ■ ■ i ■ 1 1 1 1 1 1 1 1 1 1 ' ' 1 i 1 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1329.D GCMS0208.M Fri Feb 22 09:30:12 2002 Page 1

NYC-WTC_000009832