GCMS analysis results for sample AE02568, March 2002

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Data File : C:\HPCHEM\l\DATA\MAR1902\2568.D Vial: 23 Acq On : 21 Mar 2002 2:42 am Operator: Sample : gc/ms scan 3/4 fb Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.15 0.45 ug/1 58683 1,4-Dichlorobenzene-d4 12.27

Hit# of 5 ■ Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 3-Pentanol, 2,4-dimethyl- 116 C7H160 000600-36-2 9 Abundance Scan 339 (8.154 min): 2568.D (-) m/ z 73.00 100.0 0% 73

5000 43 । । । . . f , TP - 7.80 8.00 8.20 8.40____ m/z~> ............................................... i,I ' ' I ' ' ' ' I ' ' ' ' i 1 ' ■ ' I 10 20 30 40 +L -5154 , — 50 60 70 80 I ■ ■ I • ‘ 87 103 • l ■ ■ ■ • l ■'« • • I ■ 90 100 110 m/ z 43.05 27.20% Abundance #63573: 3-Pentanol. 3-methyl- 73

5000 ■ ‘ I ‘ ■ 1 ' I '1 1 1 1 1 ' ' ' 1 1 7.80 8.00 8.20 8.40_____ 55 m/ z 41.0,5 11.57% 45 87 27 1 39, 1 1 ' i 1 ‘ ' 1 i ' ' 1 ' i 1 1 1 1 1' 11 ' 1 11 1,1 1 TT 'i 1 ------- m/z->______ 10_____ 20 .30 40 50 60 70 80 90 100 110 Abundance ■ . 51 • " - ceuno — 73 1 1 1 ' 7.80 8.00 8.20 8.40_______ 5000 m/ z 44.95 10.47% 45 15 53 59 88 m/z->........ _.. 10 ..... 20 _ Abundance 30

30 40 50 60 70 #292: N-Ethylformamide 80 90 100 110

7.80 A......— 8.00 8.20 8.40 73 m/ z 71.00 6.02% 5000 44 58

15 ----- - + । 1 1 i • 1 ' 1 i ■ ' ■ ‘ i ' 1 ' 1 i ' ■ 1 ■ i 1 ‘ ■ 1 , ' m/z--> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40

2568.D GCMS0308.M Thu Mar 21 14:20:52 2002 Page 1

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