GC/MS calibration results, PAH compounds, May 2002

Machine-extracted title · confidence 85%

GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.

NYC-WTC_000045526–000045542

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY02 0 2\94 51.D Vial: 10 Acq On 2 May 2002 11:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 3-Pentanol, 3-methyl- Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T.

8.08 0.63 ug/1 56589 1,4-Dichlorobenzene-d4 12.20

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol,/3-methyl - 102 C6H140 000077-74-7 36 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 33 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 23 4 N-Ethylformamide Abundance 7 __________ Scan 332 (8.085 min): 9451 .D (-) 73 C3H7NO 000627-45-2 9 m/z 73.10 100.00% 73

5000 43 -r-rr-rp t , ‘111‘‘1‘‘‘UUU‘’ 58 ' I ' ' I ! ! I I 7.80 8.00 8.20 8.40 4/ !jI I ! II II| I I ;Iil 87 93 103 n i11" । I i p I i i p i ! i p Ti T p i i' i p I I I p I I m/z 43.05 34.40% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.80 8.00 8.20 8.40 55 m/z 41.15 13.78% 27 45 87 1 , H39

1... .. 1 I P I I l P 11 I' I I I I I I I I I I I I I I - — I I < I P I I I P I I l P I +ttt ‘‘‘‘I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1761: Butane, 2-methoxy-2-methyl- 73 ’ 1 ‘ 1 1 ' > - I I ' ‘ 1 • I • ' 1 1 I ' ‘ . 1 7.80 8.00 8.20 8.40 5000 m/z 45.05 11.69% 55 87 45 27 33 mlz-> Abundance "i । । । । > । । । I । । । । । । i । । r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #1793: Pentane, 3-methoxy- 73 I P I I I P I I l p 11" " i

M......... 7.80 8.00 8.20 8.40 m/z 58.10 8.19% 5000 45

m/z-> 4,33,39 -+ TH 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 55 11" " I " ‘ ■ I ■ " ■ I ■' -11' ■ ■ ■ 11 ■'111 ’ >' I ■ ।

7.80 pI । । I

8.00 | r IT I

8.20 | i 1"T

8.40 । I

9451.D GCMS0501.M Fri May 03 08:42:17 2002 Page 5

NYC-WTC_000045535

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