GCMS calibration data for method 508, April 23 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2 202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise Multiplr: 1.00 MS'- Integration Params: GOOFY. P Quant Time: Apr 23 8:02 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 489831 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1782685 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.15 164 1012463 20.00 ug/1 -0.03 30) Phenanthrene-diO 25.59 188 1460641 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 961435 20.00 ug/1 -0.04 45) Perylene-dl2 37.87 264 652614 20.00 ug/1 -0.05

System Monitoring Compounds 2 8) TCMX 23.28 209 43214 8.52 ug/L -0.05 Spiked Amount 10.000 Recovery = 85.20% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00% ? Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.90 74 285 N.D. 3) bis(2-Chloroethyl)ether 11.62 93 188 N.D. 4) 1,3-Dichlorobenzene 12.11 146 490 N.D. 5) 1,4-Dichlorobenzene 12.26 146 486 N.D. 6) 1,2-Dichlorobenzene 12.77 146 461 N.D. 7) 2,21-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 14.55 82 552 N.D. 13) bis(2-Chloroethoxy)methane 15.22 93 237 N.D. 14) 1,2,4-Trichlorobenzene 15.73 180 361 N.D. 15) Naphthalene 15.89 128 1935 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.49 163 644 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 20.68 152 133 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.89 165 102 N.D. 25) Diethylphthalate 22.62 149 3647 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.77 166 347 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 23.17 168 2039 N.D. 32) 4-Bromophenyl-phenylether 24.25 248 334 N.D.

(#) = qualifier out of range (m) = manual integration 8757.D GCMS0412.M Tue Apr 23 08:05:25 2002 Page 1

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