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GCMS calibration data for method 508, April 23 2002

Machine-extracted title · confidence 100%

Calibration data for GCMS analysis of volatile organic compounds recorded on April 23, 2002.

NYC-WTC_000044313–000044337

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2202\8757.D Vial: 13 Acq On : 22 Apr 2002 8:55 pm Operator: Sample : gc/ms scan 4/11 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 23 8:02 2002 <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 790 N.D. 34) Phenanthrene 25.78 178 9313 N.D. 35) Anthracene 25.78 178 9313 0.25 ug/1 99 36) Di-n-butylphthalate 27.55 149 44365 0.94 ug/1 99 37) Fluoranthene 29.27 202 33776 0.89 ug/1. # 93 40) Pyrene 29.95 202 35862 0.93 ug/1 # 93 41) Butylbenzylphthalate 32.08 149 16849 0.89 ug/1 # 96 42) Benzo(a)anthracene 33.59 228 28765 1.07 ug/1 97 43) Bis(2-ethylhexyl)phthalate 33.86 149 49757 2.06 ug/1 99 44) Chrysene 33.71 228 28475 1.07 ug/1 97 46) Di-n-Octylphthalate 35.60 149 22558 0.59 ug/1 # 84 47) Benzo(b)fluoranthene 36.69 252 21720 0.87 ug/1 # 91 48) Benzo(k)fluoranthene 36.75 252 24356 1.00 ug/1 + 92 49) Benzo(a)pyrene 37.67 252 18332 0.89 ug/1 +: 94 50) Indeno(1,2,3-cd)pyrene 41.96 276 16136 0.78 ug/1 # 92 51) Dibenz(a,h)anthracene 42.03 278 13907 0.88 ug/1 94 52) Benzo(g,h,i)perylene 43.18 276 13429 0.78 ug/1 94

(#) = qualifier out of range (m) = manual integration 8757.D GCMS0412.M Tue Apr 23 08:05:26 2002 Page 2

NYC-WTC_000044314

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NYC-WTC_000044314Source: NYC Law Department, mirrored locally

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