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GCMS reference standard results, April 23, 2002

Machine-extracted title · confidence 100%

Reference standard analysis for GCMS testing of volatile organic compounds conducted on April 23, 2002.

NYC-WTC_000049000–000049007

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR2202\REFA2.D Vial: 18 Acq On : 23 Apr 2002 1:46 am Operator: Sample : gc/ms scan 4/12 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 23 12:25 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.68 284 166829 17.72 ug/1 98 3 4) Phenanthrene 25.65 178 758979 17.93 ug/1 99 3 5) Anthracene 25.78 178 670132 16.10 ug/1 99 36) Di-n-butylphthalate 27.55 149 938451 17.73 ug/1 99 3 7) Fluoranthene 29.28 202 753891 17.71 ug/1 96 4 0) Pyrene 29.95 202 780592 17.67 ug/1 99 41) Butylbenzylphthalate 32.09 149 336755 15.58 ug/1 96 42) Benzo(a)anthracene 33.59 228 550495 17.96 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.86 149 431289 15.60 ug/1 99 44) Chrysene 33.72 228 578820 19.04 ug/1 99 46) Di-n-Octylphthalate 35.60 149 534855 13.42 ug/1 99 47) Benzo(b)fluoranthene 36.70 252 443781 17.24 ug/1 97 48) Benzo(k)fluoranthene 36.76 252 499165 19.91 ug/1 97 4 9) Benzo(a)pyrene 37.68 252 303353 14.29 ug/1 99 50) Indeno(l,2,3-cd)pyrene 41.96 276 312636 14.63 ug/1 96 51) Dibenz(a,h)anthracene 42.02 278 276297 16.96 ug/1 99 52) Benzo(g,h,i)perylene 43.18 276 268531 15.05 ug/1 96

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Tue Apr 23 12:28:41 2002 Page 2

NYC-WTC_000049003

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NYC-WTC_000049003Source: NYC Law Department, mirrored locally

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