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GCMS reference analysis AE08209, April 2002

Machine-extracted title · confidence 100%

GCMS reference analysis report for volatile organic compounds from sample AE08209 analyzed in April 2002.

NYC-WTC_000047971–000047978

Folder label: “GCMS X 4/8/02 A 4/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1702\REFA2.D Vial: 18 Acq On : 18 Apr 2002 12:49 am Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 18 13:57 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 159917 20.67 ug/1 96 34) Phenanthrene 25.66 178 673340 19.36 ug/1 99 35) Anthracene 25.79 178 579812 16.95 ug/1 100 36) Di-n-butylphthalate 27.56 149 813062 18.68 ug/1 100 37) Fluoranthene 29.27 202 650781 18.60 ug/1 97 40) Pyrene 29.95 202 678376 19.89 ug/1 95 41) Butylbenzylphthalate 32.08 149 284830 17.07 ug/1 96 42) Benzo(a)anthracene 33.59 228 451296 19.07 ug/1 100 43) Bis(2-ethylhexyl)phthalate 33.86 149 349618 16.38 ug/1 98 44) Chrysene 33.72 228 481256 20.51 ug/1 99 46) Di-n-Octylphthalate 35.60 149 424234 13.10 ug/1 99 47) Benzo(b)fluoranthene 36.69 252 380560 18.19 ug/1 97 48) Benzo(k)fluoranthene 36.76 252 433954 21.30 ug/1 98 49) Benzo(a)pyrene 37.67 252 259985 15.07 ug/1 97 50) Indeno(1,2,3-cd)pyrene 41.95 276 324539 18.69 ug/1 95 51) Dibenz(a,h)anthracene 42.03 278 295658 22.32 ug/1 97 52) Benzo(g,h,i)perylene 43.18 276 295345 20.37 ug/1 98

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Thu Apr 18 13:59:33 2002 Page 2

NYC-WTC_000047974

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NYC-WTC_000047974Source: NYC Law Department, mirrored locally

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