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GCMS reference standard results, Sample AE05750, April 2002

Machine-extracted title · confidence 100%

Laboratory calibration data for GCMS analysis of volatile organic compounds including nitrosamines and chlorobenzenes.

NYC-WTC_000048492–000048499

Folder label: “GCMS X 4/10/02 A 4/15/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1202\REFA2.D Vial: 18 Acq On : 16 Apr 2002 12:45 am Operator: Sample : gc/ms scan 4/10 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 9:35 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Apr 16 14:55:12 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.71 284 149869 16.80 ug/1 97 34) Phenanthrene 25.67 178 650666 16.22 ug/1 99 35) Anthracene 25.81 178 570114 14.45 ug/1 100 36) Di-n-butylphthalate 27.58 149 830933 16.56 ug/1 100 37) Fluoranthene 29.30 202 634941 15.74 ug/1 97 40) Pyrene 29.98 202 659925 16.33 ug/1 97 41) Butylbenzylphthalate 32.11 149 298485 15.11 ug/1 96 42) Benzo(a)anthracene 33.61 228 434591 15.50 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.88 149 402571 15.92 ug/1 100 44) Chrysene 33.74 228 469929 16.91 ug/1 99 46) Di-n-Octylphthalate 35.62 149 497893 12.82 ug/1 100 47) Benzo(b)fluoranthene 36.71 252 369145 14.71 ug/1 99 48) Benzo(k)fluoranthene 36.78 252 405210 16.58 ug/1 99 49) Benzo(a)pyrene 37.71 252 252223 12.19 ug/1 99 50) Indeno(1,2,3-cd)pyrene 42.00 276 291775 14.00 ug/1 95 51) Dibenz(a,h)anthracene 42.08 278 251191 15.81 ug/1 99 52) Benzo(g,h,i)perylene 43.23 276 267032 15.35 ug/1 100

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0412.M Wed Apr 17 09:37:35 2002 Page 2

NYC-WTC_000048498

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NYC-WTC_000048498Source: NYC Law Department, mirrored locally

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