GCMS calibration scan data, Sample 5844, April 4 2002

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Instrument scan data for GCMS calibration using deuterated standards on April 4, 2002.

NYC-WTC_000048479–000048487

Folder label: “GCMS X 4/10/02 A 4/15/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR03022\5750.D Vial: 17 Acq On 4 Apr 2002 11:27 am Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 9 15:27 2002 Quant Results File: GCMS0408.RES

? Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 320696 20.00 ug/1 -0.02 10) Naphthalene-d8 15.88 136 1171080 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.19 164 652108 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.63 188 905494 20.00 ug/1 -0.03 39) Chrysene-dl2 33.68 240 431235 20.00 ug/1 -0.04 45) Perylene-dl2 37.92 264 230824 20.00 ug/1 -0.03 System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 30.71 235 65859 7.55 ug/mL 0.21 Spiked Amount 5.000 Recovery = 151.00% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.95 128 275 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 1074 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. (#) = qualifier out of range (m) = manual integration 5750.D GCMS0408.M Tue Apr 16 08:02:58 2002 Page 1

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