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GCMS analysis results for sample AE05847, April 17 2002

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Laboratory report documenting GCMS analysis of sample AE05847 conducted on April 17, 2002, including surrogate recovery data.

NYC-WTC_000059619–000059628

Folder label: “GCMS X 3/12/02 A 4/4/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\APR0402\5848 .D Vial: 22 Acq On 4 Apr 2002 6:47 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: GOOFY.P Quant Time: Apr 9 15:39 2002 Quant Results File: GCMS0408.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon Apr 08 11:30:53 2002 Response via : Initial Calibration DataAcq Meth : GCMS0403

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 12.24 152 332466 20.00 ug/1 -0.02 10) Naphthalene-d8 15.89 136 1209943 20.00 ug/1 -0.02 17) Acenaphthene-dlO 21.18 164 685988 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.63 188 934001 20.00 ug/1 -0.03 39) Chrysene-dl2 33.69 240 440184 20.00 ug/1 -0.03 45) Perylene-dl2 37.93 264 237887 20.00 ug/1 -0.02 System Monitoring Compounds 2 8) TCMX 0.00 209 0 0.00 ug/mL Spiked Amount 4.000 Recovery = 0.00% 38) 2,4-DDD 30.70 235 71115 7.90--ng/mL 0.20 Spiked Amount 5.000 Recoveiry Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.43 74 514 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9)' Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.93 128 325 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.67 149 918 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether- 0.00 248 0 N.D. (#) = qualifier out of range (m) = manual integration 5848.D GCMS0408.M Tue Apr 16 08:06:10 2002 Page 1

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NYC-WTC_000059621Source: NYC Law Department, mirrored locally

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