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GCMS reference analysis results for sample AE07486, April 2002

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DEP laboratory report showing GCMS reference analysis results for sample AE07486 conducted on April 20, 2002.

NYC-WTC_000047093–000047100

Folder label: “GCMS X 4/1/02 A 4/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1802\REFC2.D Vial: 16 Acq On : 20 Apr 2002 8:12 am Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 12:17 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.69 284 161526 18.93 ug/1 93 34) Phenanthrene 25.66 178 703172 18.33 ug/1 100 35) Anthracene 25.79 178 639019 16.94 ug/1 100 36) Di-n-butylphthalate 27.56 149 878730 18.31 ug/1 100 37) Fluoranthene 29.28 202 707994 18.35 ug/1 96 40) Pyrene 29.96 202 731167 17.45 ug/1 96 41) Butylbenzylphthalate 32.09 149 311773 15.22 ug/1 97 42) Benzo(a)anthracene 33.59 228 540162 18.59 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 407016 15.53 ug/1 98 44) Chrysene 33.72 228 574114 19.92 ug/1 99 46) Di-n-Octylphthalate 35.60 149 519221 12.70 ug/1 99 47) Benzo(b)fluoranthene 36.69 252 447663 16.94 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 529895 20.60 ug/1 98 49) Benzo(a)pyrene 37.68 252 329917 15.15 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.95 276 340047 15.50 ug/1 93 51) Dibenz(a,h)anthracene 42.03 278 298750 17.86 ug/1 96 52) Benzo(g,h,i)perylene 43.18 276 301163 16.45 ug/1 97

(#) = qualifier out of range (m) = manual integration REFC2.D GCMS0419.M Mon Apr 22 12:20:02 2002 Page 2

NYC-WTC_000047096

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NYC-WTC_000047096Source: NYC Law Department, mirrored locally

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