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GCMS reference analysis results for sample AE07498, April 2002

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DEP laboratory report showing GCMS reference analysis results for sample AE07498 conducted on April 19, 2002.

NYC-WTC_000047000–000047007

Folder label: “GCMS X 4/1/02 A 4/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1802\REFB1.D Vial: 4 Acq On : 19 Apr 2002 8:31 pm Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 10:28 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.69 284 146116 18.55 ug/1 93 34) Phenanthrene 25.65 178 611075 17.26 ug/1 99 35) Anthracene 25.79 178 557878 16.02 ug/1 99 36) Di-n-butylphthalate 27.56 149 722905 16.32 ug/1 100 37) Fluoranthene 29.28 202 587751 16.50 ug/1 96 40) Pyrene 29.95 202 610634 16.41 ug/1 94 41) Butylbenzylphthalate 32.08 149 246043 13.52 ug/1 96 42) Benzo(a)anthracene 33.59 228 431554 16.72 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 312558 13.42 ug/1 99 44) Chrysene 33.72 228 467380 18.26 ug/1 99 46) Di-n-Octylphthalate 35.60 149 382217 10.67 ug/1 100 47) Benzo(b)fluoranthene 36.69 252 360050 15.55 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 421676 18.70 ug/1 98 49) Benzo(a)pyrene 37.68 252 266660 13.97 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.95 276 274128 14.26 ug/1 95 51) Dibenz(a,h)anthracene 42.03 278 242898 16.57 ug/1 97 52) Benzo(g,h,i)perylene 43.17 276 237654 14.81 ug/1 98

(#) = qualifier out of range (m) = manual integration REFB1.D GCMS0419.M Mon Apr 22 10:30:30 2002 Page 2

NYC-WTC_000047006

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NYC-WTC_000047006Source: NYC Law Department, mirrored locally

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