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GCMS reference data for sample AE07484, May 2002

Machine-extracted title · confidence 90%

Reference report listing expected values for organic compounds including nitrosamines and chlorobenzenes used to validate analytical results.

NYC-WTC_000044260–000044267

Folder label: “GCMS X 4/23/02 A 4/26/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2 502\REFB1.D Vial: 4 Acq On : 26 Apr 2002 8:25 pm Operator: Sample : gc/ms scan 4/23 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 1 11:21 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Thu Apr 25 15:21:43 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 129879 18.50 ug/1 # 92 34) Phenanthrene 25.65 178 538004 17.04 ug/1 99 35) Anthracene 25.78 178 516102 16.62 ug/1 100 36) Di-n-butylphthalate 27.56 149 647072 16.39 ug/1 100 37) Fluoranthene 29.27 202 507589 15.99 ug/1 95 40) Pyrene 29.95 202 518155 17.50 ug/1 94 41) Butylbenzylphthalate 32.08 149 207003 14.30 ug/1 99 42) Benzo(a)anthracene 33.59 228 339348 16.52 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 244897 13.22 ug/1 98 44) Chrysene 33.72 228 371822 18.26 ug/1 98 46) Di-n-Octylphthalate 35.60 149 284871 10.79 ug/1 # 98 47) Benzo(b)fluoranthene 36.69 252 262145 15.37 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 329329 19.83 ug/1 98 49) Benzo(a)pyrene 37.67 252 214346 15.24 ug/1 97 50) Indeno(1,2,3-cd)pyrene 41.95 276 193002 13.63 ug/1 96 51) Dibenz(a,h)anthracene 42.02 278 165462 15.33 ug/1 96 52) Benzo(g,h,i)perylene 43.18 276 165838 14.03 ug/1 94

(#) = qualifier out of range (m) = manual integration REFB1.D GCMS0412.M Wed May 01 11:23:04 2002 Page 2

NYC-WTC_000044263

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NYC-WTC_000044263Source: NYC Law Department, mirrored locally

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