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GCMS reference standard results for sample AE06981, April 2002

Machine-extracted title · confidence 100%

Laboratory data recording the analysis of GCMS reference standards to verify instrument performance and accuracy.

NYC-WTC_000060702–000060709

Folder label: “GCMS X 3/25/02 A 4/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1802\REF2.D Vial: 7 Acq On : 18 Apr 2002 5:50 pm Operator: Sample : GC/MS SCAN 3/25 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 8:45 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\T\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17,11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 137515 13.82 ug/1 95 3 4) Phenanthrene 25.65 178 580174 12.97 ug/1 , 99 35) Anthracene 25.78 178 515182 11.71 ug/1 100 36) Di-n-butylphthalate 27.56 149 681260 12.17 ug/1 99 37) Fluoranthene 29.28 202 566389 12.59 ug/1 94 40) Pyrene 29.95 202 586184 12.76 ug/1 96 41) Butylbenzylphthalate 32.08 149 227846 10.14 ug/1 98 42) Benzo(a)anthracene 33.59 228 395568 12.42 ug/1 98 43) Bis(2-ethylhexyl)phthalate 33.86 149 402709 14.01 ug/1 98 44) Chrysene 33.72 228 439530 13.91 ug/1 99 46) Di-n-Octylphthalate 35.60 149 336954 8.07 ug/1 # 98 47) Benzo(b)fluoranthene 36.69 252 342491 12.69 ug/1 98 48) Benzo(k)fluoranthene 36.75 252 369342 14.06 ug/1 98 49) Benzo(a)pyrene 37.67 252 220412 9.91 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.95 276 227082 10.14 ug/1 96 51) Dibenz(a,h)anthracene 42.02 278 203320. 11.91 ug/1 96 52) Benzo(g,h,i)perylene 43.18 276 198062 10.59 ug/1 96

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0412.M Fri Apr 19 08:50:02 2002 Page 2

NYC-WTC_000060708

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NYC-WTC_000060708Source: NYC Law Department, mirrored locally

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