GCMS reference standard results for sample AE06981, April 2002

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1802\REF2.D Vial: 7 Acq On : 18 Apr 2002 5:50 pm Operator: Sample : GC/MS SCAN 3/25 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 19 8:45 2002 . <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table ■ Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 570838 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 2095307 20.00 ug/1 -0.03 17) Acenaphthene-di0 21.15 164 •1174908 20.00 ug/1 -0.03 30) Phenanthrene-dlO 25.59 188 1732316 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 1143228 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 706876 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 80252 3.98 ug/mL 0.16 Spiked Amount 5.000 Recovery = 79.60% Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.86 74 80938 6.51 ug/1 99 3) bis(2-Chloroethyl)ether 11.61 93 199468 10.32 ug/1 99 4) 1,3-Dichlorobenzene 12.11 146 174376 8.74 ug/1 100 5) 1,4-Dichlorobenzene 12.26 146 180984 9.02 ug/1 100 6) 1,2-Dichlorobenzene 12.77 146 179019 9.61 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.09 45 270622 10.13 ug/1 98 8) N-Nitroso-di-n-propylamine 13.47 70 129870 10.24 ug/1 99 9) Hexachloroethane 13.62 117 52886 7.19 ug/1 99 11) Nitrobenzene 13.89 77 180061 9.80 ug/1 98 12) Isophorone 14.54 82 341873 9.84 ug/1 100 13) bis(2-Chloroethoxy)methane 15.22 93 245546 10.84 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 161949 10.17 ug/1 100 15) Naphthalene 15.91 128 549155 10.90 ug/1 99 16) Hexachlorobutadiene 16.45 225 61828 7.76 ug/1 98 18) Hexachlorocyclopentadiene 18.64 237 10397 2.00 ug/1 92 19) 2-Chloronaphthalene 19.40 162 349206 11.27 ug/1 98 20) Dimethylphthalate 20.50 163 449947 12.60 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 89163 10.44 ug/1 97 22) Acenaphthylene 20.68 152 501851 11.58 ug/1 100 2 3) Acenaphthene 21.24 153 366961 11.91 ug/1 100 24) 2,4-Dinitrotoluene 21.88 165 112069 9.97 ug/1 98. 25) Diethylphthalate 22.63 149 435108 12.70 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 199519 13.12 ug/1 99 27) Fluorene 22.76 166 409419 12.55 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 375312 10.35 ug/L 94 31) N-Nitrosodiphenylamine 23.17 168 141799 9.84 ug/1 96 32) 4-Bromophenyl-phenylether 24.25 248 111782 13.29 ug/1 95 (#) = qualifier out of range (m). = manual integration REF2.D GCMS0412.M Fri Apr 19 08:50:01 2002 Page 1

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