GCMS reference results for sample AE06430, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1702\REF2.D Vial: 5 Acq On : 17 Apr 2002 12:09 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 15:37 2002 <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 448779 20.00 ug/1 -0.03 10) Naphthalene-d8 15.85 136 1586782 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.14 164 886083 20.00 ug/1 -0.03 30) Phenanthrene-diO 25.59 188 1281914 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 823109 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 532398 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 80081 5.37 ug/mL 0.17 Spiked Amount 5.000 Recovery = 107.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 83132 8.51 ug/1 97 3) bis(2-Chloroethyl)ether 11.61 93 216625 14.25 ug/1 99 4) 1,3-Dichlorobenzene 12.11 146 182759 11.66 ug/1 96 5) 1,4-Dichlorobenzene 12.26 146 187795 11.90 ug/1 98 6) 1,2-Dichlorobenzene 12.77 146 187154 12.78 ug/1 97 7) 2,21-oxybis(1-Chloropropan 13.09 45 302420 14.40 ug/1 100 8) N-Nitroso-di-n-propylamine 13.48 70 132659 13.31 ug/1 98 9) Hexachloroethane 13.62 117 50377 8.72 ug/1 97 11) Nitrobenzene 13.89 77 182848 13.14 ug/1 100 12) Isophorone 14.54 82 355905 13.52 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 260075 15.17 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 164713 13.65 ug/1 99 15) Naphthalene 15.90 128 579873 15.20 ug/1 99 16) Hexachlorobutadiene 16.44 225 56350 9.34 ug/1 99 18) Hexachlorocyclopentadiene 18.64 237 9079 2.32 ug/1 98 19) 2-Chloronaphthalene 19.40 162 354807 15.18 ug/1 99 20) Dimethylphthalate 20.49 163 443709 16.47 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 78566 12.20 ug/1 96 22) Acenaphthylene 20.68 152 505997 15.48 ug/1 100 23) Acenaphthene 21.24 153 382331 16.45 ug/1 99 24) 2,4-Dinitrotoluene 21.88 165 92845 10.95 ug/1 99 25) Diethylphthalate 22.62 149 426114 16.49 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 204899 17.87 ug/1 98 27) Fluorene 22.76 166 416995 16.94 ug/1 96 29) Azobenzen/ 1,2-Diphenylhyd 23.25 77 362035 13.24 ug/L 96 31) N-Nitrosodiphenylamine 23.17 168 108093 10.14 ug/1 98 32) 4-Bromophenyl-phenylether 24.25 248 110294 17.72 ug/1 95

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0412.M Wed Apr 17 15:39:05 2002 Page 1

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