GCMS reference results for sample AE05845, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR2302\REFA1.D Vial: 17 Acq On : 24 Apr 2002 5:59 am Operator: Sample : gc/ms scan 4/17 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 24 11:16 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 531076 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1928409 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1101893 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.59 188 1629488 20.00 ug/1 -0.02 39) Chrysene-dl2 33.64 240 1085865 20.00 ug/1 -0.03 45) Perylene-dl2 37.88 264 678830 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 23.29 209 48481 8.78 ug/L -0.04 Spiked Amount 10.000 Recovery = 87.80% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.86 74 104702 9.06 ug/1 95 3) bis(2-Chloroethyl)ether 11.61 93 253887 14.11 ug/1 100 4) 1,3-Dichlorobenzene 12.11 146 210053 11.32 ug/1 99 5) 1,4-Dichlorobenzene 12.25 146 222786 11.93 ug/1 100 6) 1,2-Dichlorobenzene 12.77 146 219247 12.65 ug/1 99 7) 2,21 -oxybis(l-Chloropropan 13.09 45 352486 14.18 ug/1 99 8) N-Nitroso-di-n-propylamine 13.47 70 166619 14.12 ug/1 98 9) Hexachloroethane 13.62 117 64713 9.46 ug/1 95 11) Nitrobenzene 13.89 77 230151 13.61 ug/1 99 12) Isophorone 14.54 82 382319 11.95 ug/1 99 13) bis(2-Chloroethoxy)methane 15.22 93 304927 14.63 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 197597 13.48 ug/1 98 15) Naphthalene 15.90 128 683117 14.73 ug/1 100 16) Hexachlorobutadiene 16.45 225 73538 10.03 ug/1 96 18) Hexachlorocyclopentadiene 18.64 237 5979 1.23 ug/1 96 19) 2-Chloronaphthalene 19.40 162 430286 14.81 ug/1 97 20) Dimethylphthalate 20.50 163 540723 16.14 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 113388 14.16 ug/1 96 22) Acenaphthylene 20.67 152 615665 15.14 ug/1 100 23) Acenaphthene 21.24 153 447399 15.48 ug/1 100 24) 2,4-Dinitrotoluene 21.87 165 144053 13.66 ug/1 96 25) Diethylphthalate 22.63 149 520282 16.19 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 238039 16.69 ug/1 98 27) Fluorene 22.76 166 498046 16.27 ug/1 98 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 461377 13.57 ug/L 99 31) N-Nitrosodiphenylamine 23.17 168 149807 11.05 ug/1 98 32) 4-Bromophenyl-phenylether 24.24 248 133001 16.81 ug/1 98

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0412.M Wed Apr 24 11:16:20 2002 Page 1

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