GCMS reference analysis results for sample AE07498, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1802\REFB2.D Vial: 5 Acq On : 19 Apr 2002 9:29 pm Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 10:30 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 485589 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1775128 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 1015344 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1500409 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 1027396 20.00 ug/1 -0.03 45) Perylene-dl2 37.88 264 697041 20.00 ug/1 -0.04

System Monitoring Compounds 28) TCMX 23.29 209 41379 4.89 ug/L -0.04 Spiked Amount 4.000 Recovery = 122.25% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 95795 9.06 ug/1 99 3) bis(2-Chloroethyl)ether 11.60 93 232608 14.14 ug/1 99 4) 1,3-Dichlorobenzene 12.11 146 226120 13.33 ug/1 99 5) 1,4-Dichlorobenzene 12.26 146 231739 13.58 ug/1 98 6) 1,2-Dichlorobenzene 12.77 146 223878 14.12 ug/1 99 7) 2,21 -oxybis(1-Chloropropan 13.09 45 319958 14.08 ug/1 98 8) N-Nitroso-di-n-propylamine 13.48 70 151874 14.08 ug/1 98 9) Hexachloroethane 13.62 117 81350 13.01 ug/1 95 11) Nitrobenzene 13.89 77 208941 13.43 ug/1 99 12) Isophorone 14.54 82 384412 13.05 ug/1 98 13) bis(2-Chloroethoxy)methane 15.22 93 283654 14.79 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 206475 15.30 ug/1 98 15) Naphthalene 15.90 128 641956 15.04 ug/1 99 16) Hexachlorobutadiene 16.45 225 105298 15.60 ug/1 96 18) Hexachlorocyclopentadiene 18.64 237 23392 5.21 ug/1 99 19) 2-Chloronaphthalene 19.41 162 408520 15.26 ug/1 98 20) Dimethylphthalate 20.49 163 548362 17.76 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 112865 15.29 ug/1 97 22) Acenaphthylene 20.67 152 598391 15.97 ug/1 100 23) Acenaphthene 21.24 153 429015 16.11 ug/1 100 24) 2,4-Dinitrotoluene 21.88 165 145718 15.00 ug/1 98 25) Diethylphthalate 22.63 149 527080 17.80 ug/1 100 26) 4-Chlorophenyl-phenylether 22.78 204 240522 18.31 ug/1 97 27) Fluorene 22.76 166 486726 17.26 ug/1 97 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 445514 14.22 ug/L 98 31) N-Nitrosodiphenylamine 23.17 168 163988 13.14 ug/1 100 32) 4-Bromophenyl-phenylether 24.24 248 136661 18.76 ug/1 96

(#) = qualifier out of range (m) = manual integration REFB2.D GCMS0419.M Mon Apr 22 10:32:21 2002 Page 1

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