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GCMS reference results for sample AE06430, April 2002

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Laboratory report documenting GCMS reference analysis of sample AE06430 conducted on April 17, 2002.

NYC-WTC_000039445–000039452

Folder label: “GCMS X 3/19/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1702\REF2.D Vial: 5 Acq On : 17 Apr 2002 12:09 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 17 15:37 2002 <Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue

33) Hexachlorobenzene 24.68 284 135433 18.39 ug/1 99 34) Phenanthrene 25.65 178 576517 17.41 ug/1 100 35) Anthracene 25.79 178 499497 15.34 ug/1 99 36) Di-n-butylphthalate 27.56 149 687044 16.59 ug/1 99 37) Fluoranthene 29.28 202 558974 16.78 ug/1 94 4 0) Pyrene 29.95 202 575304 17.40 ug/1 98 41) Butylbenzylphthalate 32.08 14 9 237476 14.69 ug/1 99 42) Benzo(a)anthracene 33.58 228 380364 16.58 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 299508 14.48 ug/1 98 44) Chrysene 33.71 228 418711 18.41 ug/1 100 46) Di-n-Octylphthalate 35.60 149 342620 10.89 ug/1 99 47) Benzo(b)fluoranthene 36.69 252 329581 16.22 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 363792 18.39 ug/1 98 49) Benzo(a)pyrene 37.67 252 216766 12.94 ug/1 99 50) Indeno(1,2,3-cd)pyrene 41.96 276 277356 16.44 ug/1 98 51) Dibenz(a,h)anthracene 42.03 278 245206 19.06 ug/1 97 52) Benzo(g,h,i)perylene 43.18 276 249687 17.73 ug/1 99

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0412.M Wed Apr 17 15:39:06 2002 Page 2

NYC-WTC_000039448

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NYC-WTC_000039448Source: NYC Law Department, mirrored locally

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