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GCMS reference analysis AE08209, April 2002

Machine-extracted title · confidence 100%

GCMS reference analysis report for volatile organic compounds from sample AE08209 analyzed in April 2002.

NYC-WTC_000047971–000047978

Folder label: “GCMS X 4/8/02 A 4/18/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR17O2\REFA1.D Vial: 17 Acq On : 17 Apr 2002 11:51 pm Operator: Sample : gc/ms scan 4/8 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 18 13:54 2002 Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.68 284 134419 19.02 ug/1 97 34) Phenanthrene 25.65 178 548879 17.28 ug/1 99 35) Anthracene 25.78 178 466935 14.94 ug/1 100 36) Di-n-butylphthalate 27.55 149 682724 17.18 ug/1 99 37) Fluoranthene 29.28 202 530870 16.61 ug/1 94 40) Pyrene 29.95 202 551339 18.61 ug/1 96 41) Butylbenzylphthalate 32.08 149 222344 15.35 ug/1 98 42) Benzo(a)anthracene 33.58 228 356447 17.35 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 276619 14.92 ug/1 98 44) Chrysene 33.71 228 381277 18.71 ug/1 99 46) Di-n-Octylphthalate 35.60 149 325010 11.14 ug/1 # 98 47) Benzo(b)fluoranthene 36.69 252 310735 16.48 ug/1 98 4 8) Benzo(k)fluoranthene 36.75 252 332540 18.11 ug/1 97 4 9) Benzo(a)pyrene 37.67 252 215248 13.85 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.95 276 259203 16.56 ug/1 96 51) Dibenz(a,h)anthracene 42.02 278 226206 18.95 ug/1 98 52) Benzo(g,h,i)perylene 43.17 276 242330 18.55 ug/1 99

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0412.M Thu Apr 18 13:57:28 2002 Page 2

NYC-WTC_000047977

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NYC-WTC_000047977Source: NYC Law Department, mirrored locally

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