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GCMS reference standard results, April 23, 2002

Machine-extracted title · confidence 100%

Reference standard analysis for GCMS testing of volatile organic compounds conducted on April 23, 2002.

NYC-WTC_000049000–000049007

Folder label: “GCMS X 4/12/02 A 4/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\APR22O2\REFA1.D Vial: 17 Acq On : 23 Apr 2002 12:48 am Operator: Sample : gc/ms scan 4/12 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 23 12:14 2002 Quant Results File: GCMS0412.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Compound R.T. Qlon Response Cone Unit Qvalue 33) Hexachlorobenzene 24.68 284 158948 16.91 ug/1 98 3 4) Phenanthrene 25.65 178 725509 17.17 ug/1 100 35) Anthracene 25.78 178 639774 15.39 ug/1 lob 36) Di-n-butylphthalate 27.56 149 934922 17.68 ug/1 100 37) Fluoranthene 29.28 202 724992 17.06 ug/1 94 40) Pyrene 29.95 202 757109 16.79 ug/1 99 41) Butylbenzylphthalate 32.08 149 332333 15.07 ug/1 99 4 2) Benzo(a)anthracene 33.59 228 549759 17.57 ug/1 99 43) Bis(2-ethylhexyl)phthalate 33.86 149 438630 15.54 ug/1 99 44) Chrysene 33.72 228 574335 18.52 ug/1 99 46) Di-n-Octylphthalate 35.60 149 545946 12.74 ug/1 99 47) Benzo(b)fluoranthene 36.70 252 455054 16.43 ug/1 98 48) Benzo(k)fluoranthene 36.76 252 526252 19.52 ug/1 98 4 9) Benzo(a)pyrene 37.68 252 318766 13.96 ug/1 98 50) Indeno(1,2,3-cd)pyrene 41.96 276 337213 14.67 ug/1 96 51) Dibenz(a,h)anthracene 42.03 278 303894 17.34 ug/1 95 52) Benzo(g,h,i)perylene 43.19 276 291567 15.19 ug/1 97

(#) = qualifier out of range (m) = manual integration REFAl.D GCMS0412.M Tue Apr 23 12:16:28 2002 Page 2

NYC-WTC_000049006

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NYC-WTC_000049006Source: NYC Law Department, mirrored locally

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