GCMS reference analysis results for sample AE07498, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\APR1802\REFB1.D Vial: 4 Acq On : 19 Apr 2002 8:31 pm Operator: Sample : gc/ms scan 4/1 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 22 10:28 2002 Quant Results File: GCMS0419.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0419.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Apr 19 14:51:24 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 444084 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1594321 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 921906 20.00 ug/1 -0.02 30) Phenanthrene-dlO 25.59 188 1371133 20.00 ug/1 -0.03 39) Chrysene-dl2 33.65 240 926379 20.00 ug/1 -0.03 45) Perylene-dl2 37.87 264 606567 20.00 ug/1 -0.05

System Monitoring Compounds 2 8) TCMX 23.29 209 37570 4.89 ug/L -0.04 Spiked Amount 4.000 Recovery = 122.25% 38) 2,4-DDD 0.00 235 0 0.00 ug/mL Spiked Amount 5.000 Recovery = 0.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.87 74 91608 9.48 ug/1 97 3) bis(2-Chloroethyl)ether 11.60 93 219077 14.56 ug/1 100 4) 1,3-Dichlorobenzene 12.11 146 217456 14.02 ug/1 100 5) 1,4-Dichlorobenzene 12.26 146 221639 14.20 ug/1 100 6) 1,2-Dichlorobenzene 12.77 146 213606 14.74 ug/1 99 7) 2,21-oxybis(1-Chloropropan 13.09 45 297303 14.30 ug/1 99 8) N-Nitroso-di-n-propylamine 13.48 70 139520 14.14 ug/1 98 9) Hexachloroethane 13.62 117 77725 13.59 ug/1 98 11) Nitrobenzene 13.89 77 195757 14.00 ug/1 99 12) Isophorone 14.54 82 348191 13.17 ug/1 97 13) bis(2-Chloroethoxy)methane 15.22 93 264080 15.33 ug/1 99 14) 1,2,4-Trichlorobenzene 15.73 180 192698 15.90 ug/1 99 15) Naphthalene 15.90 128 605785 15.80 ug/1 99 16) Hexachlorobutadiene 16.45 225 99493 16.41 ug/1 98 18) Hexachlorocyclopentadiene 18.64 237 21878 5.37 ug/1 98 19) 2-Chloronaphthalene 19.41 162 381318 15.68 ug/1 98 20) Dimethylphthalate 20.49 163 481226 17.17 ug/1 99 21) 2,6-Dinitrotoluene 20.71 165 95695 14.28 ug/1 96 22) Acenaphthylene 20.67 152 545139 16.03 ug/1 99 23) Acenaphthene 21.24 153 390402 16.15 ug/1 100 24) 2,4-Dinitrotoluene 21.88 165 124398 14.10 ug/1 99 25) Diethylphthalate 22.63 149 451153 16.78 ug/1 99 26) 4-Chlorophenyl-phenylether 22.78 204 217858 18.26 ug/1 99 27) Fluorene 22.76 166 441179 17.23 ug/1 97 29) Azobenzen/ 1,2-Diphenylhyd 23.24 77 390227 13.72 ug/L 94 31) N-Nitrosodiphenylamine 23.17 168 148256 13.00 ug/1 97 32) 4-Bromophenyl-phenylether 24.24 248 120685 18.13 ug/1 97

(#) = qualifier out of range (m) = manual integration REFB1.D GCMS0419.M Mon Apr 22 10:30:29 2002 Page 1

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