GCMS analysis results for sample AE06454, April 2002

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Laboratory report documenting GCMS analysis of sample AE06454 conducted on April 19, 2002, by the DEP.

NYC-WTC_000039574–000039587

Folder label: “GCMS X 3/19/02 A 4/17/02”

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Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\APR1702\6454.D Vial: 12 Acq On : 17 Apr 2002 6:59 pm Operator: Sample : gc/ms scan 3/19 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 18 9:03 2002 ।Quant Results File: GCMS0412.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Apr 17 11:48:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0412

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.21 152 437186 20.00 ug/1 -0.03 10) Naphthalene-d8 15.84 136 1560928 20.00 ug/1 -0.03 17) Acenaphthene-diO 21.15 164 860237 20.00 ug/1 -0.02 30) Phenanthrene-diO 25.58 188 1195698 20.00 ug/1 -0.03 39) Chrysene-dl2 33.64 240 665445 20.00 ug/1 -0.04 45) Perylene-dl2 37.87 264 419964 20.00 ug/1 -0.05

System Monitoring Compounds 28) TCMX 0.00 209 0 0.00 ug/L Spiked Amount 10.000 Recovery = 0.00% 38) 2,4-DDD 30.66 235 79263 5.69 ug/mL 0.16 Spiked Amount 5.000 Recovery = 113.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.49 74 281 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.89 128 466 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.57 165 201 N.D. 25) Diethylphthalate 22.63 149 2443 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D.

(#) = qualifier out of range (m) = manual integration 6454.D GCMS0412.M Thu Apr 18 09:04:04 2002 Page 1

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GCMS analysis results for sample AE06453, April 2002 · Box DEP Box 23

NYC-WTC_000039560

Laboratory report documenting GCMS analysis of sample AE06453 conducted on April 19, 2002, by the DEP.

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