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GCMS analysis results for sample AE02599, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02599 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005302–000005311

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005309
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAR0102\2599.D Vial: 9 Acq On 1 Mar 2002 4:14 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.35 ug/1 27145 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 4 3 1,3-Dioxolane , 2- (1-methylpropyl) - 130 C7H14O2 014447-25-7 4 4 Formic acid, ethyl ester 74 C3H602 000109-94-4 4 Abundance / Scan 343 (8.195 min): 2599.D (-) m/ z 73.00 1 00.00% • 73

5000 43 _ —.............. 1 1 1 1 1 11 I ' 1 ' 1 I I I I I I I I 7.80 8.00 8.20 32-8.60 8.40 07% ri ।1 >>1111 ■ 111 ,1149 57 .... ,i 1 ' ' i ' 1 37 i 1 ' 1 i ' ' ' 1 i 1 ' ' 1 1 1 1 1 1 1 1 ' 1 m/ z 42.95 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #63573: 3-Pentanol, 3-methyl- 73 ...................

5000 7.80 8.00 8.20 8.40 8.60 . 45 55 87 m/ z 45.05 12.56% 27 39, 1 ' 1 i 1 1 ■ ' i 1 1 1 ' i ' ' ‘ ' T' I’Iu ! 'j■■। ।■■■.।i।i।।।।>■ii'।>।।।।■।ii।।।>। m/Z-2____ 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance ' 30 73 7.80_ 8.00 8.20 8.40 8.60 5000 m/z 41.05 ' 10.61% 44 58

15 ’IIInnIIbnII**,***/ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #5441: 1,3-Dioxolane, 2-(1-methylpropyl)- 73 7.80 8.00__ 8.20__ 8.40 8.60 m/z 71.00 6.95% 5000

45 27 | 57 ,85 99 1 29 ' ' i ' ' ' ' i ' ' ■ ' i 1 1 ' 1 i ■ ■ ■ 1 i 1 t’t’v i ' ' 1 ' 1 1 1 1 1 1 1 ' 1 ' 1 1 ' 1 ' I T 1 1 I 1 ' ' 1 I ' 1 1 ''I 1 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 7.80 8.00 8.20 8.40 8.60

2599 .D GCMS0208.M Mon Mar 04 11:43:29 2002 Page 1

NYC-WTC_000005309

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NYC-WTC_000005309Source: NYC Law Department, mirrored locally

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