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GCMS analysis results for sample AE02599, Mar 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02599 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005302–000005311

Folder label: “GCMS X 2/5/02 A 3/1/02

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Scanned page image, NYC-WTC_000005310
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2599.D Vial: 9 Acq On 1 Mar 2002 4:14 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.23 ug/1 25017 Phenanthrene-dl0 25.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-d10 • z 2 3H-Naphtho[1,8/bc]thiophen-3-one, 4 -7 4 188 188 C14D10 C11H8OS 001517-22-2 010245-79-1 10 9 3 Anthracene-d1- 188 C14D10 001719-06-8 9 4 4-Methyl-2-(3-fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 7 Abundance Z ■ 2 ** er (25.849 Scan 2266 min):' " '' 2599.D (-) m/z188.10100.00% 188

5000 /........... 94 ' 1 I 1 1 1 1 1 ' ’ 1 1 1 1 1 1 1 I 1 1 66 80 156

m/z~> 44 TIII+’II’t 40 50 60 ml 80 90 100p 70 TIf II — m/Z 110 120 130 140 150 160 170 180 190 TT ... 25.60 25.80 26.00 26.20 94.00 21.82% Abundance #19958: Phenanthrene-did 188

— 5000 25.60 25.80 26.00 26.20 m/ z 65.95 12.99% 66 80 94 160 ' ' I " . ... 1............................................ m । m । । । m/z->____ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 183 / 3-1 1 1 1 ' ' i 1 ■ ■ • i ' ' 25.60 25.80 26.00 26.20 5000 m/z 156.05 11.19% 115 160 63 89 128 145 171 m/z~> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d 10- -- 188 25.60 25.80 26.00 26.20 m/ z 80.05 10.24% 5000

80 94 160 66 ■ ■ i ■r > ■ i ■ > ■ > ।

40 50 60 ■ 111 ■

70 —. la— - 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2599.D GCMS0208.M Mon Mar 04 11:43:34 2002 Page 2

NYC-WTC_000005310

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NYC-WTC_000005310Source: NYC Law Department, mirrored locally

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