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GCMS analysis results for sample AE05897, March 29 2002

Machine-extracted title · confidence 100%

Laboratory report detailing GCMS analysis of environmental sample AE05897 conducted on March 29, 2002.

NYC-WTC_000059755–000059766

Folder label: “GCMS X 3/13/02 A 3/27/02

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Scanned page image, NYC-WTC_000059762
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\5897.D Vial: 25 Acq On : 22 Mar 2002 12:56 pm Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Phenanthrene-dlO ■ Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.21 ug/1 80617 Phenanthrene-dl0 25.67

Hit# of Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 78 2 Anthrace dlO- 188 C14D10 001719-06-8 53 3 4-Methyl (3 - fluorophenyl)pyrimidi 188 C11H9FN2 076128-66-0 53 4 5(4H)-Iqbxazolone, 4,4'-bis[3-methy 376 C22H20N2O4 000000-00-0 40 Abundance Scan“22^ (257^ m/z 188710 1 !8

5000

80 94 42 52 66 I ,l 106 25.40 25.60 25.80 26.00 26,20 rrrt+krtTTtTT 136 146 170 1,1 7't~r+T-YT-TrT-p-rl4^pTTT--r1-TT-TT-|-t444Y''-rT-r-| m/z 80.05 15.36% 30 40 50 60 70 80 90. 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-diO.................................... ' 1$8

5000 n i ' ' 25.40 25.60 25.80 26.00 26.20 160 m/z 189.10 13.82% 66 94 I ..... rTir ’m/z-> 30 40 50 60 70 80 90 100 110 120 W 140 150 J60_ 170 180 190 Abundance Anthracenc-dKJ- 188 r-r-T-J- 25.40 25.60 25.80 26.00 26.20 5000 m/ Z 94.00 13.57%

Rc 80 94 160

zL 66 I ‘ ‘ ' I ' ' ' ' I m/z->__ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19859:4-Methyl-2-(3-fluorophenyl)pyrimidine 188 25.40 25.60 25.80 26.00 26.20 11.22% 5000 121

67 173 94 I 146 161 I fn/2-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

5897.D GCMS0308.M Mon Mar 25 14:27:17 2002 Page 1

NYC-WTC_000059762

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NYC-WTC_000059762Source: NYC Law Department, mirrored locally

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