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GCMS blank analysis results for sample AE01156, March 25 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS blank analysis results for sample AE01156 conducted on March 25, 2002, with compound detection limits.

NYC-WTC_000059670–000059678

Folder label: “GCMS X 3/13/02 A 3/27/02

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Scanned page image, NYC-WTC_000059676
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\LBA.D Vial: 16 Acq On : 22 Mar 2002 2:05 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.21 ug/1 57466 Phenanthrene-dl0 25.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO ' 188 C14D10 001517-22-2 80 2 Anthracene-dlO- 188 C14D10 001719-06-8 53 3 4-Fluoro-6.-methyl-2-phenylpyrimidin 188 C11H9FN2 000000-00-0 36 4 Benzene, I-(1-cyclohexen-l-yl)-4-me 188 C13H16O 020758-60-5 9 Abundance ' “ ' ' . ..... ” Scan 22^(20oi riiinyLBADlH......................... 1fi8 m/z 188710 TooTod’?

5000

94 42 m/z->.......... 40 I.......Ph ,,, I 50 60 70 80 h+u 132 146 ,160 90 100 110 120 130 140 150 160 170 180 190 2A4O_25.6O_^JO 26^ 26.20 m/z 189.10 16‘. 44%' Abundance #19958: Phenanthrene-dlO 188

5000 . l\ . • 25.40 25.60 25.80 26.00 26.20 80 .160 I' m/z 94.00 12.48% 94 ... I. . ....... I, ...... I, m/z->40__ 50 60 70 80 An- 90 10p_ l10_120_i30_140’ 150 160 170 180 190 Abundance #19957: Arndracon&/d 1(1 .......... "" 188 1 T 25.40 25.60 25.80 26.00 26.20 5000 m/z 80.05 11.43%

80 94 160 66 I 11 CQ^“h_ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19858: 4-Fiuoro-6-methyi-2-phenyipyrimidine 1 1 88 25.40 25.60 25.80 26.00 26.20 m/z 184.10 10.39% 5000 85 103 51 77 94 173 I il 114 I p-n-q-m-r-j- II V ' I ' ' 40 50 60 70 80 i90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

LBA.D GCMS0308.M Mon Mar 25 14:30:22 2002 Page 1

NYC-WTC_000059676

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NYC-WTC_000059676Source: NYC Law Department, mirrored locally

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