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GCMS analysis results for sample AE01156, March 29 2002

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Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.

NYC-WTC_000059693–000059702

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR2102\1156.D Vial: 19 Acq On 22 Mar 2002 5:02 am Operator: Sample re-extract Inst, : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.80 0.21 ug/1 61420 Phenanthrene-dl0 25.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-c^lO 188 C14D10 001517-22-2 56 2 4-Methyl-2-(y^fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 42 3 3-Quinolinecarbonitrile, 1,2,3,4-te 188 C10H8N2O2 022384-05-0 40 4 Anthracene-dlO- 188 C14D10 001719-06-8 40 Abundancs. .... .. .. ’ .... ..Scanli^'i (25799 min): 1156.D {-) 1f'.8

5000

155 25.40 25.60 25.80 26.00 26.20 40 54 66 108 132 ■ ■ >' I' I' 1111111111 .11 'O'"........ . m/z 189.10 11.90% m/z->30 40.. 50..... 60.. 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanfhrene-d i 0 188

5000 25.40 25.60 25.80 26.00 26.20 80 m/z 94.00 11.25% 94 160 66 I , I II m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19«?0 4-Me1hyl-;>M-f!L jrop'iy!!v’,p/!. rtdint 188

121 25.40 25.60 25.80 26.00 26.20 5000 m/z 184.10 9.83% 173 67 94 57 75 102 146 , I . . I I , I . . 1 L , I , m/z-> 30 40 50 60 70 I80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19815; 3-Quinolinecarbonitrile, 1,2,3,4-tetrahydro-1-hydro 1f!8 25.40 25.60 25.80 26.00 26.20 m/z 80.00 8.12% 128 172 93 5000 117 142 66

m/z-> 30 40 50 60 70 80 A 17 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 26.20

1156.D GCMS0308.M Mon Mar 25 14:22:26 2002 Page 1

NYC-WTC_000059700

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NYC-WTC_000059700Source: NYC Law Department, mirrored locally

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