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GCMS analysis results for sample AE01156, March 29 2002

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Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.

NYC-WTC_000059693–000059702

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR21O2\1156.D Vial: 19 Acq On : 22 Mar 2002 5:02 am Operator: . Sample : re-extract Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Isopropyl Palmitate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 0.69 ug/1 203919 Phenanthrene-dl0 25.66

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Isopropyl Palrnitate 298 C19H38O2 000142-91-6 46 2 Hexadecanoic ,acid 256 C16H32O2 000057-10-3 35 3 Nonanoic acid 158 C9H18O2 000112-05-0 18 4 _alpha. -D-Galactopyranosidej, -y methyl 194 C7H14O6 P03396-99-4 17 Abundance /■ Scan 2517 (28.149 min): 1156.D(-) 4l3

60 102 5000 73 83 129 239 256 A m/Z“>........... 40 60 Km 80.. 100 115 120 140 I 143 157 171 185 199 213 227 1610 180 ; 200.. 220.. 240 I 260 27.80 28.00 28.20 28.40 m/z 60.05 62.97% Abundance #42488: isopropyl Palmitate 162

5000 60 73 129 27.80 28.00 28.20 28.40 m/z" 101.9 5 62.66% 157 257 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #7160" Hexa'Jecano.c flcic 43 60 73 i I 27.80 28.00 28.20 28.40 5000 256 m/z " 41'. 05 51.68% 129

.. i n T i 157 171 I 213 I 227 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #67434: Nonanoic acid ......................... ...................................... ** 73 27.80 28.00 28.20 28.40 m/z 5'7-0,0 48.06% 5000

'm/z-> 40 , ,1.1. , ,1 60 87 f '7 129 l|l, , A, , ,1, , , ,1... 1,58.................. 80 100 120 140 160 180 200 220 240 260 27.80 28.00 28.20 28.40 1 I "n

1156.D GCMS0308.M Mon Mar 25 14:22:30 2002 Page 2

NYC-WTC_000059701

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NYC-WTC_000059701Source: NYC Law Department, mirrored locally

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