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GCMS analysis results for sample AE05896, March 29 2002

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Laboratory report detailing GCMS analysis of environmental sample AE05896 conducted on March 29, 2002.

NYC-WTC_000059745–000059754

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2102\5896.D Vial: 24 Acq On : 22 Mar 2002 11:57 am Operator: Sample : gc/ms scan 3/13 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Isopropyl Palmitate Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

28.15 0.37 ug/1 129447 Phenanthrene-dl0 25.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Isopropyl Palmity4te 298 C19H38O2 000142-91-6 38 2 Hexadecanoic acid 256 C16H32O2 000057-10-3 30 3 Isopropyl 3-methylbutanoate 144 C8H16O2 000000-00-0 12 4 Nonanoic acid 158 C9H18O2 000112-05-0 10 Abundance . Scan 2517 (28.149 min): 5896.D (-) m/z” ”4 3” OS..... 10 0 700 % 40 A 60 102

5000 256 73 I I 82 129 911 239 ■R

J, 115 I 143 157 171 185 199 227 I 27.80 28.00 28.20 28.40 m/z 102.05' 69.02% m/z-;^ 40...W... 80.. 100.. 120.. .... 160 180 200 220 240 260 Abundance #42488: isopropyl Palmitate i 102

5000 60 73 129 27.80 28.00 28.20 28.40 85 m/z 60.05 65.78% !. 157 257 I m/z-> 40 6.Q..8O 100 120 140 160 180 200 220 240 260 Abundance #35'.SC. Hexadecanoic acid i 43 60 7 27.80 28.00 28.20 28.40 5000 m/z 41.0,5 55.46% 85 97 129 213 I i 157 171 185 256 :mfe--> Abundance 40 60 80 1.00__ 120.. 140.. 160 180 ' 200 220 ' ' 240 ’ ' 260 #8368: isopropyl 3-methyibulanoate' 1 27.80 28.00 28.20 .„28AO_____ 60 85 m/z 57.0.0 ’ 48.11% 5000 103 j, , t|. . . . , .1 I . , 1^9 , , , .. m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 27.80 28.00 28.20 28.40

5896.D GCMS0308.M Mon Mar 25 14:26:11 2002 Page 2

NYC-WTC_000059753

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NYC-WTC_000059753Source: NYC Law Department, mirrored locally

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